3,3'-亚氨基二丙酸二乙酯合成路线 （共 23 条）
反应条件
palladium 10 on activated carbon; ammonium formate in ethanol 2 h; Reflux;
参考文献
Lu, Guo-Liang; Stevenson, Ralph J.; Chang, John Yu-Chih; Brothers, Penelope J.; Ware, David C.; Wilson, William R.; Denny, William A.; Tercel, Moana
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 16 p. 4861 - 4867
反应条件
1: With ammonium hydroxide; hydroxylamine hydrochloride in ethanol T=20°C; 15 h; 2: With indium; ammonium chloride in ethanol 7.5 h; Heating;
参考文献
Cicchi, Stefano; Bonanni, Marco; Cardona, Francesca; Revuelta, Julia; Goti, Andrea
Organic Letters, 2003 , vol. 5, # 10 p. 1773 - 1776
参考文献
Hahn, Ekkehardt F.; Rupprecht, Stefan
Chemische Berichte, 1991 , vol. 124, # 3 p. 481 - 486
反应条件
ammonium hydroxide; palladium in tetrahydrofuran T=65°C; Suzuki coupling; 6 h;
参考文献
Buchmeiser, Michael R.; Schareina, Thomas; Kempe, Rhett; Wurst, Klaus
Journal of Organometallic Chemistry, 2001 , vol. 634, # 1 p. 39 - 46
参考文献
Kuettel; McElvain
Journal of the American Chemical Society, 1931 , vol. 53, p. 2692,2696
Full Text Show Details
Chodroff; Kapp; Beckmann
Journal of the American Chemical Society, 1947 , vol. 69, p. 256
反应条件
1: aqueous Ba(OH)2 2: HCl View Scheme
参考文献
Chodroff; Kapp; Beckmann
Journal of the American Chemical Society, 1947 , vol. 69, p. 256
参考文献
Aventis Pharma Limited
Patent: US6352977 B1, 2002 ;
Location in patent: Page column 98 ;
反应条件
1: sulfuric acid / Reflux; Inert atmosphere 2: 10 palladium on activated charcoal; ammonium formate / methanol View Scheme
参考文献
He, Dongsheng; He, Gu; Guo, Li
Letters in Organic Chemistry, 2011 , vol. 8, # 7 p. 454 - 460
参考文献
Dickerman; Lindwall
Journal of Organic Chemistry, 1949 , vol. 14, p. 530,534
参考文献
Hromatka; Eiles
Monatshefte fuer Chemie, 1948 , vol. 78, p. 137
