2'-羟基-3-苯基苯丙酮合成路线 （共 38 条）
反应条件
aluminium trichloride 1 h;
参考文献
Alvaro, Mercedes; Baldovi, Vicenta; Garcia, Hermenegildo; Miranda, Miguel, A.; Primo, Jaime
Monatshefte fuer Chemie, 1990 , vol. 121, # 4 p. 267 - 274
反应条件
sodium hydroxide; palladium on activated charcoal Hydrogenation;
参考文献
Act chim.hung., , vol. 13, p. 217,225
Pharmaceutica Acta Helvetiae, , vol. 34, p. 241,243
反应条件
1: 54 percent / N-chlorosuccinimide, pyridine / CHCl3 / 2 h / Heating 2: 14 percent / H2, boric acid / Raney-Ni / methanol; H2O View Scheme
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 42, # 5 p. 303 - 308
反应条件
1: 54 percent / N-chlorosuccinimide, pyridine / CHCl3 / 2 h / Heating 2: 14 percent / H2, boric acid / Raney-Ni / methanol; H2O View Scheme
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 42, # 5 p. 303 - 308
反应条件
1: 57 percent / KOH / ethanol; H2O / 10 h / Ambient temperature 2: 801 mg / H2 / Adams catalyst / ethyl acetate / 0.17 h / 2068.6 Torr / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1567 - 1577
反应条件
1: 57 percent / KOH / ethanol; H2O / 10 h / Ambient temperature 2: 801 mg / H2 / Adams catalyst / ethyl acetate / 0.17 h / 2068.6 Torr / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1567 - 1577
反应条件
1: 1.) LDA / 1.) THF, 0 deg C to 25 deg C, 1 h, 2.) THF, -50 deg C to 25 deg C 2: 89 percent / AcOH / tetrahydrofuran; H2O / 4 h / 40 °C View Scheme
参考文献
Tetrahedron, , vol. 54, # 51 p. 15711 - 15720
反应条件
1: 1.) LDA / 1.) THF, 0 deg C to 25 deg C, 1 h, 2.) THF, -50 deg C to 25 deg C 2: 89 percent / AcOH / tetrahydrofuran; H2O / 4 h / 40 °C View Scheme
参考文献
Tetrahedron, , vol. 54, # 51 p. 15711 - 15720
反应条件
1: CHCl3 2: 84 percent / AlCl3 / 1 h View Scheme
参考文献
Monatshefte fuer Chemie, , vol. 121, # 4 p. 267 - 274
反应条件
1: SOCl2 / CHCl3 / 2 h / Heating 2: CHCl3 3: 84 percent / AlCl3 / 1 h View Scheme
参考文献
Monatshefte fuer Chemie, , vol. 121, # 4 p. 267 - 274
