4,4,5,5,6,6,7,7-八氢二苯并四硫富瓦烯合成路线 (共 12 条)
反应条件
triethylamine in tetrahydrofuran T=25°C;
参考文献
Fabre, J. M.; Giral, L.; Gouasmia, A.; Cristau, H. J.; Ribeill, Y.
Bulletin de la Societe Chimique de France, 1987 , # 5 p. 823 - 826
反应条件
triethyl phosphite T=130°C; 24 h; Inert atmosphere;
参考文献
Inoue, Jun-Ichi; Kanno, Masato; Ashizawa, Minoru; Seo, Chayeon; Tanioka, Akihiko; Mori, Takehiko
Chemistry Letters, 2010 , vol. 39, # 6 p. 538 - 540
反应条件
dicobalt octacarbonyl in toluene 1 h;
参考文献
Coustumer, Gerard Le; Mollier, Yves
Journal of the Chemical Society, Chemical Communications, 1980 , # 1 p. 38 - 39
反应条件
1: acetone / 3 h 2: sulfuric acid / 3 h / Cooling with ice 3: triethyl phosphite / 24 h / 130 °C / Inert atmosphere View Scheme
参考文献
Inoue, Jun-Ichi; Kanno, Masato; Ashizawa, Minoru; Seo, Chayeon; Tanioka, Akihiko; Mori, Takehiko
Chemistry Letters, 2010 , vol. 39, # 6 p. 538 - 540
反应条件
1: sulfuric acid / 3 h / Cooling with ice 2: triethyl phosphite / 24 h / 130 °C / Inert atmosphere View Scheme
参考文献
Inoue, Jun-Ichi; Kanno, Masato; Ashizawa, Minoru; Seo, Chayeon; Tanioka, Akihiko; Mori, Takehiko
Chemistry Letters, 2010 , vol. 39, # 6 p. 538 - 540
反应条件
triethylamine 2.) -80 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Giral, L.; Fabre, J. M.; Gouasmia, A.
Tetrahedron Letters, 1986 , vol. 27, # 36 p. 4315 - 4318
反应条件
triethylamine 2.) -80 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Giral, L.; Fabre, J. M.; Gouasmia, A.
Tetrahedron Letters, 1986 , vol. 27, # 36 p. 4315 - 4318
参考文献
Gimbert; Moradpour; Bittner
Tetrahedron Letters, 1990 , vol. 31, # 7 p. 1007 - 1010
参考文献
Gimbert; Moradpour; Bittner
Tetrahedron Letters, 1990 , vol. 31, # 7 p. 1007 - 1010
参考文献
Fabre, J. M.; Giral, L.; Gouasmia, A.; Cristau, H. J.; Ribeill, Y.
Bulletin de la Societe Chimique de France, 1987 , # 5 p. 823 - 826