1,1,1-三氟-3-苯基丙酮合成路线 （共 31 条）
反应条件
trifluorormethanesulfonic acid in dichloromethane T=0 - 20°C; 12.1667 h; Inert atmosphere;
参考文献
Tetrahedron, , vol. 69, # 31 p. 6448 - 6460
反应条件
in diethyl ether T=20°C; Grignard reaction; 0.5 h;
参考文献
Grunewald, Gary L.; Caldwell, Timothy M.; Li, Qifang; Criscione, Kevin R.
Journal of Medicinal Chemistry, 1999 , vol. 42, # 17 p. 3315 - 3323
反应条件
pyridine in dichloromethane T=-60°C; 8.5 h;
参考文献
Boivin, Jean; El Kaim, Laurent; Zard, Samir Z.
Tetrahedron Letters, 1992 , vol. 33, # 10 p. 1285 - 1288
反应条件
Dess-Martin periodane in dichloromethane 3 h; Ambient temperaturevariation in ratios of reagent and reaction times; Product distribution;
参考文献
Linderman, Russell J.; Graves, David M.
Journal of Organic Chemistry, 1989 , vol. 54, # 3 p. 661 - 668
反应条件
hydrogen fluoride in dichloromethane 2 h; Ambient temperature;
参考文献
Begue, J. P.; Mesureur, D.
Journal of Fluorine Chemistry, 1988 , vol. 39, p. 271 - 282
反应条件
tribenzylzinnchlorid in diethyl ether 0.5 h;
参考文献
Greif, Dieter; Riedel, Dirk; Feindt, Andreas; Pulst, Manfred
Journal fuer Praktische Chemie/Chemiker-Zeitung, 1995 , vol. 337, # 1 p. 34 - 37
反应条件
sodium hydride in tetrahydrofuran 3 h; Inert atmosphereRefluxSchlenk technique;
参考文献
Yang, Dongmei; Zhou, Yuhan; Xue, Na; Qu, Jingping
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 4171 - 4176
反应条件
in diethyl ether T=0°C; 1 h;
参考文献
Gais; Jungen; Jadhav
Journal of Organic Chemistry, 2001 , vol. 66, # 10 p. 3384 - 3396
反应条件
sulfuric acid; water
参考文献
Journal of the American Chemical Society, , vol. 72, p. 5409,5412
