1,2-二(2-氟苯基)乙烷合成路线 （共 7 条）
参考文献
Aitken, R. Alan; Hodgson, Philip K. G.; Oyewale, Adebayo O.; Morrison, John J.
Chemical Communications, 1997 , # 13 p. 1163 - 1164
参考文献
Aitken, R. Alan; Hodgson, Philip K. G.; Oyewale, Adebayo O.; Morrison, John J.
Chemical Communications, 1997 , # 13 p. 1163 - 1164
反应条件
1: With 2,2,6,6-tetramethyl-piperidine; n-butyllithium; potassium tert-butylate in tetrahydrofuran T=-78°C; 0.25 h; Inert atmosphere; 2: With ethylene dibromide in tetrahydrofuran T=-78 - 20°C; Inert atmosphere; regioselective reaction;
参考文献
Blangetti, Marco; Fleming, Patricia; O'Shea, Donal F.
Journal of Organic Chemistry, 2012 , vol. 77, # 6 p. 2870 - 2877
反应条件
magnesium 1.) THF, reflux, 1 h, 2.) THF, RT, 4 d; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Corey, Joyce Y.; Pitts, Alexander J.; Winter, Rudolph E.K.; Rath, Nigam P.
Journal of Organometallic Chemistry, 1995 , vol. 499, # 1.2 p. 113 - 122
反应条件
magnesium 1.) THF, reflux, 1 h, 2.) THF, reflux, overnight; Yield given. Multistep reaction;
参考文献
Corey, Joyce Y.; Pitts, Alexander J.; Winter, Rudolph E.K.; Rath, Nigam P.
Journal of Organometallic Chemistry, 1995 , vol. 499, # 1.2 p. 113 - 122
反应条件
magnesium T=600°C; P=1.1 Torr; Product distribution; Further Variations:Pressures;
参考文献
Aitken, R. Alan; Hodgson, Philip K.G.; Morrison, John J.; Oyewale, Adebayo O.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 3 p. 402 - 415
反应条件
magnesium T=600°C; P=1 Torr; Product distribution; Further Variations:Pressures;
参考文献
Aitken, R. Alan; Hodgson, Philip K.G.; Morrison, John J.; Oyewale, Adebayo O.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 3 p. 402 - 415
