4-硝基苄基4-硝基苯甲酸酯合成路线 (共 17 条)
反应条件
phenylmethanethiol; phenyl-magnesium bromide in tetrahydrofuran; diethyl ether T=65°C; Tishchenko reaction; 18 h; Inert atmosphere;
参考文献
Cronin, Linda; Manoni, Francesco; O'Connor, Cornelius J.; Connon, Stephen J.
Angewandte Chemie - International Edition, 2010 , vol. 49, # 17 p. 3045 - 3048
反应条件
trifluoromethylsulfonic anhydride; N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C; 2 h;
参考文献
Mahdavi, Hossein; Amani, Javad
Tetrahedron Letters, 2008 , vol. 49, # 14 p. 2204 - 2207
反应条件
2,4,6-trimethyl-pyridine; hydrogen; chlorohydridotris(triphenylphosphine)ruthenium in toluene T=55°C; P=760 Torr; 24 h;
参考文献
Grushin, Vladimir V.; Alper, Howard
Journal of Organic Chemistry, 1991 , vol. 56, # 17 p. 5159 - 5161
反应条件
potassium carbonate; butanone; amino alcohol-based Ir bifunctional catalyst T=20°C; 48 h;
参考文献
Suzuki, Takeyuki; Matsuo, Tomohito; Watanabe, Kazuhiro; Katoh, Tadashi
Synlett, 2005 , # 9 art. no. U05305ST, p. 1453 - 1455
反应条件
La[N(TMS)2]3 in benzene-d6 T=25°C; 24 h;
参考文献
Seo, SungYong; Marks, Tobin J.
Organic Letters, 2008 , vol. 10, # 2 p. 317 - 319
反应条件
tetrabutylammomium bromide; sodium hydrogencarbonate; sodium iodide in acetonitrile T=80°C; 8 h;
参考文献
Hu; Pa; Cui; Wang
Synthetic Communications, 1992 , vol. 22, # 19 p. 2763 - 2767
反应条件
manganese(IV) oxide; oxygen; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1,3-bis(2,4,6-trimethylphenyl)imidazolinium chloride in tetrahydrofuran T=50°C; 24 h;
参考文献
Xin, Yang-Chun; Shi, Shi-Hui; Xie, Dong-Dong; Hui, Xin-Ping; Xu, Peng-Fei
European Journal of Organic Chemistry, 2011 , # 32 p. 6527 - 6531
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in water T=80°C; 6 h;
参考文献
Majji, Ganesh; Guin, Srimanta; Gogoi, Anupal; Rout, Saroj Kumar; Patel, Bhisma K.
Chemical Communications, 2013 , vol. 49, # 29 p. 3031 - 3033
反应条件
iodine; potassium carbonate in tert-butyl alcohol T=50°C; 27 h;
参考文献
Tumkevicius; Navickas; Dailide
Polish Journal of Chemistry, 2006 , vol. 80, # 8 p. 1377 - 1383
反应条件
sodium hydroxide in tetrahydrofuran T=20°C; 0.25 h;
参考文献
Pandi, Muthupandi; Chanani, Prem Kumar; Govindasamy, Sekar
Applied Catalysis A: General, 2012 , vol. 441-442, p. 119 - 123