4-甲氧基-2-甲基-1-丁烯合成路线 (共 6 条)
反应条件
Cp2Ti(OTf)2 in CD3NO2 T=25°C;
参考文献
Hollis, T. Keith; Robinson, N. P.; Whelan, John; Bosnich, B.
Tetrahedron Letters, 1993 , vol. 34, # 27 p. 4309 - 4312
反应条件
barium sulfate T=300°C;
参考文献
Fischer,W.; Grob,C.A.
Helvetica Chimica Acta, 1978 , vol. 61, p. 2336 - 2350
反应条件
1: 2-methyl-4-hydroxy-1-butene With sodium hydride in triglyme (triethylene glycol dimethyl ether) 2: methyl iodide
参考文献
Bowen, Richard D.; Edwards, Howell G.M.; Varnali, Tereza
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2012 , vol. 93, p. 26 - 32
反应条件
nitric acid T=55 - 60°C; 5 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Arakelyan, A. S.; Dvoryanchikov, A. I.; Gevorkyan, A. A.
Journal of Organic Chemistry USSR (English Translation), 1985 , p. 1193 - 1196
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 6 p. 1311 - 1314
反应条件
bis(η3-allyl-μ-chloropalladium(II)); tributylphosphine; sodium methylate in isopropyl alcohol 4 h; Ambient temperaturevariable katalysator-system; Product distribution;
参考文献
Gaube, W.; Stegemann, H.
Journal fuer Praktische Chemie (Leipzig), 1984 , vol. 326, # 6 p. 947 - 954
反应条件
aluminum oxide; copper phosphate aluminium oxide T=310°C; P=60 Torr;
参考文献
Comp.d'Alais
Patent: US2561483 , 1949 ;