呋喃并[2,3-b]吡啶-5-胺合成路线 （共 5 条）
反应条件
hydrogen; palladium on activated charcoal in benzene T=25°C; 0.75 h;
参考文献
Yamaguchi, Seiji; Kurosaki, Masahide; Yokoyama, Hajime; Hirai, Yoshiro; Shiotani, Shunsaku
Journal of Heterocyclic Chemistry, 1998 , vol. 35, # 6 p. 1305 - 1307
反应条件
1: quinoline / Cu / 3 h / 185 - 200 °C 2: H2 / Pd-C / benzene / 0.75 h / 25 °C View Scheme
参考文献
McFarland,J.W. et al.
Journal of Heterocyclic Chemistry, 1971 , vol. 8, p. 735 - 738
反应条件
hydrogenchloride; sodium cyanide; sodium nitrite 1.) from 0 deg C to 5 deg C, 15 min, 2.) benzene, RT, 3 h; Yield givenMultistep reaction;
参考文献
Yamaguchi, Seiji; Kurosaki, Masahide; Yokoyama, Hajime; Hirai, Yoshiro; Shiotani, Shunsaku
Journal of Heterocyclic Chemistry, 1998 , vol. 35, # 6 p. 1305 - 1307
反应条件
1: 1.) 35 percent aq. HCl, NaNO2, 2.) aq. NaCN / 1.) from 0 deg C to 5 deg C, 15 min, 2.) benzene, RT, 3 h 2: 33 percent / DIBAL-H / CH2Cl2 / 0.25 h / -50 °C View Scheme
参考文献
Yamaguchi, Seiji; Kurosaki, Masahide; Yokoyama, Hajime; Hirai, Yoshiro; Shiotani, Shunsaku
Journal of Heterocyclic Chemistry, 1998 , vol. 35, # 6 p. 1305 - 1307
反应条件
hydrogen bromide; copper(I) bromide; sodium nitrite 1.) 0 deg C, 15 min; Yield givenMultistep reaction;
参考文献
Yamaguchi, Seiji; Kurosaki, Masahide; Yokoyama, Hajime; Hirai, Yoshiro; Shiotani, Shunsaku
Journal of Heterocyclic Chemistry, 1998 , vol. 35, # 6 p. 1305 - 1307
