反应条件
1: n-butyl-magnesium chloride With 1,4-bis(2,4,6-trimethylphenyl)-1,2,3-triazol-3-ium iodide in tetrahydrofuran
T=0°C; 0.5 h;
2: (2E,4E)-1-chlorohexa-2,4-diene T=20°C; 4 h; Overall yield = 99percent;
参考文献
Nomura, Ryosuke; Tsuchiya, Yuji; Ishikawa, Hiroyuki; Okamoto, Sentaro
Tetrahedron Letters, 2013 , vol. 54, # 11 p. 1360 - 1363