反应条件
carbon monoxide in tetrahydrofuran
High Pressure; 0.05 mmol Pd compound, 0.1 mmol Et2Zn, 2.5 ml THF, CO 30 atm (at -50°), stirred at 25°C for 2 h in presence of 0.2 mmol MgClBr, (yield of PhCEt(OH)COEt/PhCOCEt2(OH): 68percent), previous product ratio for previous conditions; GC-MS, GC;
参考文献
Yamashita, Hiroshi; Kobayashi, Toshi-aki; Sakakura, Toshiyasu; Tanaka, Masato
Journal of Organometallic Chemistry, 1988 , vol. 356, p. 125 - 132
