3-甲基-2-苯并呋喃-1(3H)-酮合成路线 (共 49 条)
反应条件
[bis(acetoxy)iodo]benzene; potassium bromide in dichloromethane T=40°C; 8 h;
参考文献
Dohi, Toshifumi; Takenaga, Naoko; Goto, Akihiro; Maruyama, Akinobu; Kita, Yasuyuki
Organic Letters, 2007 , vol. 9, # 16 p. 3129 - 3132
反应条件
carbonylchlorohydridetris(triphenylphosphine) ruthenium(II) in toluene T=120°C; 40 h; Inert atmosphere;
参考文献
Omura, Sohei; Fukuyama, Takahide; Murakami, Yuji; Okamoto, Hiromi; Ryu, Ilhyong
Chemical Communications, 2009 , # 44 p. 6741 - 6743
反应条件
potassium hydroxide; sodium tetrahydroborate
参考文献
Tobia, David; Rickborn, Bruce
Journal of Organic Chemistry, 1986 , vol. 51, # 20 p. 3849 - 3858
反应条件
4-(N,N-dimethlyamino)pyridine; 1,1'-bis-(diphenylphosphino)ferrocene; N-ethyl-N,N-diisopropylamine; palladium diacetate in 1,4-dioxane T=180°C; 0.5 h; microwave irradiation;
参考文献
Wu, Xiongyu; Mahalingam; Wan, Yiqian; Alterman, Mathias
Tetrahedron Letters, 2004 , vol. 45, # 24 p. 4635 - 4638
反应条件
copper(II) bis(trifluoromethanesulfonate); triphenylphosphine; ruthenium trichloride; silver trifluoromethanesulfonate in acetonitrile T=80°C; 96 h;
参考文献
Ohta, Tetsuo; Kataoka, Yohei; Miyoshi, Akio; Oe, Yohei; Furukawa, Isao; Ito, Yoshihiko
Journal of Organometallic Chemistry, 2007 , vol. 692, # 1-3 p. 671 - 677
反应条件
sodium methylate; C2H5OOCCH2Co(CO)4 in methanol T=25°C;
参考文献
Foa, M.; Francalanci, F.; Bencini, E.; Gardano, A.
Journal of Organometallic Chemistry, 1985 , vol. 285, p. 293 - 304
反应条件
hydrogenchloride; n-butyllithium in tetrahydrofuran; hexane; ethyl acetate
参考文献
Allergan, Inc.
Patent: US2004/19098 A1, 2004 ;
反应条件
in N,N-dimethyl-formamide 13 h; Inert atmosphereReflux;
参考文献
COUNCIL OF SCIENTIFIC and INDUSTRIAL RESEARCH; REDDY, Santhosh, Rekula; PRAGATI, Kishore, Prasad; NAGA, Kiran, Chaithanya, Indukuru; SUDALAI, Arumugam
Patent: WO2013/102935 A2, 2013 ;
Location in patent: Page/Page column 19 ;
反应条件
[Cp*Ir(6,6’-(OH)2bpy)(H2O)][OTf]2; sodium hydrogencarbonate in water 6 h; Inert atmosphereRefluxGreen chemistry;
参考文献
Fujita, Ken-Ichi; Ito, Wataru; Yamaguchi, Ryohei
ChemCatChem, 2014 , vol. 6, # 1 p. 109 - 112
反应条件
hydrogenchloride; water T=20°C; 48 h;
参考文献
Mangas-Sanchez, Juan; Busto, Eduardo; Gotor-Fernandez, Vicente; Gotor, Vicente
Organic Letters, 2012 , vol. 14, # 6 p. 1444 - 1447