N-(1-金刚烷)甲酰胺合成路线 （共 19 条）
反应条件
1: formic acid With acetic anhydride T=20°C; 1 h; Inert atmosphereSchlenk technique; 2: 1-adamantaneamine in dichloromethane T=-78 - 20°C; Inert atmosphereSchlenk technique;
参考文献
Martin, David; Lassauque, Nicolas; Steinmann, Florian; Manuel, Gerald; Bertrand, Guy
Chemistry - A European Journal, 2013 , vol. 19, # 44 p. 14895 - 14901
反应条件
styrene; [Ru(η4-COD)(η3-methylallyl)2]; potassium tert-butylate; ICy*HCl in toluene T=125°C; 24 h; Inert atmosphereGlovebox;
参考文献
Ortega, Nuria; Richter, Christian; Glorius, Frank
Organic Letters, 2013 , vol. 15, # 7 p. 1776 - 1779
反应条件
trifluoroacetic acid T=90 - 95°C; 8 h;
参考文献
Shokova; Musulu, Tasula; Luzikov; Kovalev
Russian Journal of Organic Chemistry, 1999 , vol. 35, # 6 p. 844 - 856
反应条件
triethylamine in tetrahydrofuran T=65°C; 45 h; Inert atmosphereSchlenk technique;
参考文献
Shintani, Ryo; Nozaki, Kyoko
Organometallics, 2013 , vol. 32, # 8 p. 2459 - 2462
反应条件
Formylation; 12 h; Heating;
参考文献
Ronsisvalle, Giuseppe; Marrazzo, Agostino; Prezzavento, Orazio; Pasquinucci, Lorella; Falcucci, Barbara; Di Toro, Rosanna; Spampinato, Santi
Bioorganic and Medicinal Chemistry, 2000 , vol. 8, # 6 p. 1503 - 1513
反应条件
T=200 - 220°C; 0.0333333 h; Heating;
参考文献
Isaev, S. D.; Novoselov, E. F.; Yurchenko, A. G.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 1 p. 103 - 108
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 1 p. 114 - 119
反应条件
sulfuric acid 18 h; Ambient temperature;
参考文献
Chen; Goel; Kesten; Knobelsdorf
Tetrahedron Letters, 1996 , vol. 37, # 45 p. 8129 - 8132
反应条件
sulfuric acid 18 h; Ambient temperature;
参考文献
Chen; Goel; Kesten; Knobelsdorf
Tetrahedron Letters, 1996 , vol. 37, # 45 p. 8129 - 8132
反应条件
1: tricyclo[3.3.1.1{3,7}]decane With sulfuric acid; nitric acid T=0°C; 18 h; 2: formamide T=0 - 20°C; Ritter-type reaction; 2.5 h; Further stages.;
参考文献
Wanka, Lukas; Cabrelle, Chiara; Vanejews, Maksims; Schreiner, Peter R.
European Journal of Organic Chemistry, 2007 , # 9 p. 1474 - 1490
反应条件
1: 28.6 percent / peroxyacetic acid / CH2Cl2 / 2 h / 0 - 5 °C 2: 93.5 percent / 0.03 h / 200 - 220 °C / Heating View Scheme
参考文献
Druelinger,M.L. et al.
Journal of Heterocyclic Chemistry, 1976 , vol. 13, p. 1001 - 1007
