(Z)-11-十六碳烯-1-乙酸盐合成路线 （共 74 条）
反应条件
pyridine 12 h; Ambient temperature;
参考文献
Odinokov, V. N.; Akhmetova, V. R.; Khasanov, Kh. D.; Abduvakhabov, A. A.; Tolstikov, G. A.
Chemistry of Natural Compounds, 1991 , vol. 27, # 1 p. 116 - 118
Khimiya Prirodnykh Soedinenii, 1991 , # 1 p. 132 - 135
反应条件
in acetic acid T=35 - 40°C;
参考文献
Vig, O. P.; Sharma, M. L.; Vohra, Neelam; Sabharwal, Arun; Huq, M. A.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 1069 - 1070
反应条件
pyridine in benzene 4 h; Heating;
参考文献
Singh; Misra
Journal of the Indian Chemical Society, 1990 , vol. 67, # 7 p. 565 - 567
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Seidel, Wolfgang; Schaefer, Hans J.
Chemische Berichte, 1980 , vol. 113, # 12 p. 3898 - 3903
反应条件
pyridine; acetic anhydride
反应条件
1: HMPA / tetrahydrofuran 2: p-toluenesulfonic acid / methanol 3: H2 / Pd/BaSO4 4: pyridine View Scheme
参考文献
Pesticide Science, , vol. 41, # 2 p. 97 - 103
反应条件
1: ethylmagnesium bromide / diethyl ether / 3.5 h / Heating 2: diethyl ether / 4 h / 0 - 2 °C 3: 79 percent / pyridine / 1.) -5 deg C, 6 h; 2.) 0 deg C, 12 h 4: 53 percent / sodium iodide, zinc dust / tetrahydrofuran / 1.) 65-70 deg C, 3 h; 2.) 20 deg C, 3 h 5: 1.) 2percent O3 in O2; 2.) sodium tetrahydroborate / 1.) cyclohexane, methanol; 2.) room temp., 15 h 6: 1.) isobutylmagnesium bromide; 2.) C5H5TiCl2 / 1.) diethyl ether, 0 deg C, 15 min; 2.) room temp., 1-1,5 h 7: 90 percent / pyridine View Scheme
参考文献
Chemistry of Natural Compounds, , vol. 23, # 3 p. 365 - 368
Khimiya Prirodnykh Soedinenii, , # 3 p. 440 - 444
反应条件
1: HMPA / tetrahydrofuran 2: p-toluenesulfonic acid / methanol 3: H2 / Pd/BaSO4 4: pyridine View Scheme
参考文献
Pesticide Science, , vol. 41, # 2 p. 97 - 103
反应条件
1: p-toluenesulfonic acid / methanol 2: H2 / Pd/BaSO4 3: pyridine View Scheme
参考文献
Pesticide Science, , vol. 41, # 2 p. 97 - 103
反应条件
1: 1.) Na2SO3, NaHCO3 / 1.) H2O, 10 h, 2.) 1 h 2: Et3N / CH2Cl2 / 1 h / Ambient temperature 3: 1.) Mg / 1.) Et2O, 2.) reflux, 1 h 4: (AcO)2Cu / acetic acid; H2O / 0.67 h / Heating 5: 85percent hydrazine hydrate / butan-1-ol / Heating 6: O2, CuCl / pyridine 7: acetic acid / 10 h / 50 °C 8: H2 / P-2 Ni View Scheme
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 329, # 2 p. 283 - 289
反应条件
1: Et3N / CH2Cl2 / 1 h / Ambient temperature 2: 1.) Mg / 1.) Et2O, 2.) reflux, 1 h 3: (AcO)2Cu / acetic acid; H2O / 0.67 h / Heating 4: 85percent hydrazine hydrate / butan-1-ol / Heating 5: O2, CuCl / pyridine 6: acetic acid / 10 h / 50 °C 7: H2 / P-2 Ni View Scheme
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 329, # 2 p. 283 - 289
