4,4-二溴二苯基二硫化物合成路线 （共 34 条）
反应条件
copper(l) iodide; Na2S*9H2O; potassium carbonate in N,N-dimethyl-formamide T=120°C; 18 h; Inert atmosphere; chemoselective reaction;
参考文献
Li, Yaming; Nie, Caiping; Wang, Huifeng; Li, Xiaoying; Verpoort, Francis; Duan, Chunying
European Journal of Organic Chemistry, 2011 , # 36 p. 7331 - 7338
反应条件
[2,2']bipyridinyl; copper(l) iodide; sulfur; magnesium chloride in N,N-dimethyl-formamide T=110°C; 40 h; Product distribution; Further Variations:Reagentstime;
参考文献
Taniguchi, Nobukazu
Tetrahedron, 2012 , vol. 68, # 51 p. 10510 - 10515,6
反应条件
Cu/Al2O3; potassium carbonate in N,N-dimethyl-formamide T=110°C;
参考文献
Bhadra, Sukalyan; Sreedhar, Bojja; Ranu, Brindaban C.
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 14-15 p. 2369 - 2378
反应条件
dihydrogen peroxide; bromine in dichloromethane; water 6 h;
参考文献
Ye, Jun; Chen, Zhan; Fung, Man-Keung; Zheng, Caijun; Ou, Xuemei; Zhang, Xiaohong; Yuan, Yi; Lee, Chun-Sing
Chemistry of Materials, 2013 , vol. 25, # 13 p. 2630 - 2637
反应条件
chloro-trimethyl-silane; sodium bromide in acetonitrile 1) r.t., 20 min, 2) 40 deg C, 30 min;
参考文献
Schmidt, Arthur H.; Russ, Manuel
Chemische Berichte, 1981 , vol. 114, # 3 p. 1099 - 1110
反应条件
bromine in dichloromethane; water
参考文献
Thackeray, James W.; Coley, Suzanne M.; Cameron, James F.; LaBeaume, Paul J.; Madkour, Ahmad E.; Ongayi, Owendi; Jain, Vipul
Patent: US2012/141939 A1, 2012 ;
反应条件
zinc in carbonic acid dimethyl ester T=80°C; 0.416667 h; Microwave irradiation;
参考文献
Kundu, Debasish; Ahammed, Sabir; Ranu, Brindaban C.
Green Chemistry, 2012 , vol. 14, # 7 p. 2024 - 2030
反应条件
trifluoroacetic acid in 1,4-dioxane T=110°C; 15 h;
参考文献
Wagner, Anna M.; Sanford, Melanie S.
Journal of Organic Chemistry, 2014 , vol. 79, # 5 p. 2263 - 2267
反应条件
acetic acid beim Bromieren;
参考文献
Bravo; Dordi; Fontana; Minisci
Journal of Organic Chemistry, 2001 , vol. 66, # 9 p. 3232 - 3234
反应条件
sodium hydroxide; sulfuric acid; sodium acetate; copper; sodium nitrite in water 1) 0 - 5 deg C, 1 h, 2) 60 - 70 deg C, 105 min;
参考文献
Jilek, Jiri; Pomykacek, Josef; Holubek, Jiri; Svatek, Emil; Ryska, Miroslav; et al.
Collection of Czechoslovak Chemical Communications, 1984 , vol. 49, # 3 p. 603 - 620
