甲基(2E,4E,6E,8E)-3,7-二甲基-9-(2,6,6-三甲基-1-环己烯基)壬-2,4,6,8-四烯酸酯合成路线 （共 32 条）
参考文献
Julia,M.; Arnould,D.
Bulletin de la Societe Chimique de France, 1973 , p. 746 - 750
参考文献
Julia,M.; Arnould,D.
Bulletin de la Societe Chimique de France, 1973 , p. 746 - 750
参考文献
BASF
Patent: DE950552 , 1954 ;
反应条件
1: acetic acid; aqueous sulfuric acid; petroleum ether 2: zinc; ethyl acetate; benzene 3: oxalic acid / unter vermindertem Druck View Scheme
参考文献
Inhoffen et al.
Justus Liebigs Annalen der Chemie, 1950 , vol. 568, p. 52,62
Chemische Berichte, 1951 , vol. 84, p. 361,366
反应条件
1: KOtBu 2: NaOMe View Scheme
参考文献
Julia,M.; Arnould,D.
Bulletin de la Societe Chimique de France, 1973 , p. 746 - 750
反应条件
2: KOtBu 3: NaOMe View Scheme
参考文献
Julia,M.; Arnould,D.
Bulletin de la Societe Chimique de France, 1973 , p. 746 - 750
反应条件
1: KOtBu 2: NaOMe View Scheme
参考文献
Julia,M.; Arnould,D.
Bulletin de la Societe Chimique de France, 1973 , p. 746 - 750
反应条件
2,3,5-trimethyl-pyridine; silica gel; silver nitrate 1.) acetonitrile; 2.) column chromatography with hexane-ether; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Solladie, G.; Berl, V.
Bulletin de la Societe Chimique de France, 1993 , vol. 130, p. 568 - 574
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Warner and Co. Inc.
Patent: DE828543 , 1948 ;
DRP/DRBP Org.Chem.
Full Text Show Details
Robeson et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 4111,4117
反应条件
1: 80.3 percent / m-chloroperbenzoic acid, NaHCO3 / CH2Cl2; H2O / 1 h / ice bath 2: 63.7 percent / 10percent KOH / H2O / 1 h View Scheme
参考文献
Matsui; Kajiwara; Hatanaka; Waldmann; Schreier
Bioscience, Biotechnology and Biochemistry, 1994 , vol. 58, # 1 p. 140 - 145
