in diethyl ether a Grignard soln. (prepd. from MeI and Mg in Et2O) is added to the suspn. of InCl3 in ether and refluxed for 3 h; distn. of excess of Et2O at atm. pressure affords Me3In*Et2O; repeated distn. of the etherate at room temp. in vac. affords InMe3;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 7 - 12
