n,n-二甲基亚甲基碘化胺合成路线 （共 57 条）
反应条件
potassium carbonate in toluene 5 h; Ambient temperature;
参考文献
Pochini, Andrea; Puglia, Giuseppe; Ungaro, Rocco
Synthesis, 1983 , # 11 p. 906 - 907
参考文献
Greco, Michael N.; Hawkins, Michael J.; Powell, Eugene T.; Almond Jr., Harold R.; De Garavilla, Lawrence; Hall, Jeffrey; Minor, Lisa K.; Wang, Yuanping; Corcoran, Thomas W.; Di Cera, Enrico; Cantwell, Angelene M.; Savvides, Savvas N.; Damiano, Bruce P.; Maryanoff, Bruce E.
Journal of Medicinal Chemistry, 2007 , vol. 50, # 8 p. 1727 - 1730
反应条件
sodium hydride in tetrahydrofuran Heating;
参考文献
Heterocycles, , vol. 46, # 1 p. 65 - 70
反应条件
acetic acid in methanol T=25°C; 4 h; Inert atmosphere;
参考文献
Soto, Sara; Vaz, Esther; Dell'Aversana, Carmela; Alvarez, Rosana; Altucci, Lucia; De Lera, Angel R.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 10 p. 2101 - 2112
反应条件
AgNO2 in acetonitrile T=25°C; 16 h; stirred with silver nitrate in acetonitrile, in THF; Product distribution;
参考文献
Boyer, Joseph H.; Pillai, T. Perumal
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1661 - 1664
反应条件
methanesulfonic acid; sulfuric acid in chloroform-d1 T=20 - 70°C; 3 h; screw-capped test-tube; Product distribution / selectivity;
参考文献
Loctite (RandD) Limited; Universita Degli Studi di Parma
Patent: US7718821 B1, 2010 ;
Location in patent: Page/Page column 7 ;
反应条件
Yield given. Multistep reaction;
参考文献
Ley, Steven V.; Trudell, Mark L.; Wadsworth, David J.
Tetrahedron, 1991 , vol. 47, # 38 p. 8285 - 8296
反应条件
16 h; Ambient temperature; Yield given;
参考文献
Mann, Robert K.; Parsons, Jack G.; Rizzacasa, Mark A.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 7 p. 1283 - 1293
反应条件
ammonium hydroxide; water 1) 1 h, CH2Cl2, -70 deg C, 2) 0 deg C, pH= 12; Yield given. Multistep reaction;
参考文献
Risch, Nikolaus; Esser, Achim
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1989 , vol. 44, # 2 p. 208 - 210
反应条件
zinc in acetonitrile 1) cooling with an ice-salt bath -> room temperature, 5 h, 2) room temp., 2 days;
参考文献
Journal of Organic Chemistry, , vol. 48, # 10 p. 1621 - 1628
