(2Z)-3-氯-3-苯基-2-丙烯醛合成路线 （共 23 条）
参考文献
Ziegenbein; Franke
Angewandte Chemie, 1959 , vol. 71, p. 573
反应条件
toluene-4-sulfonic acid T=110 - 112°C; 0.0333333 h; microwave irradiation;
参考文献
Synthetic Communications, , vol. 32, # 23 p. 3541 - 3547
反应条件
1: 85 percent / ethanolic HCl / 2 h / Ambient temperature 2: 56.9 percent / 0.05 h / 220 - 250 °C View Scheme
参考文献
Roy; Kar; Ray
Synthetic Communications, 1993 , vol. 23, # 14 p. 1959 - 1965
反应条件
in diethyl ether T=0°C; Cyclization; 3 h; Heating;
参考文献
Pavlik, James W.; Kebede, Naod
Journal of Organic Chemistry, 1997 , vol. 62, # 24 p. 8325 - 8334
反应条件
in diethyl ether T=0°C; Cyclization; 3 h; Heating;
参考文献
Pavlik, James W.; Kebede, Naod
Journal of Organic Chemistry, 1997 , vol. 62, # 24 p. 8325 - 8334
反应条件
1: β-chloro cinnamaldehyde With sodium sulfide nonahydrate in N,N-dimethyl-formamide T=60°C; 2 h; 2: chloroacetone in N,N-dimethyl-formamide T=60°C; 3 h; 3: With potassium carbonate in water; N,N-dimethyl-formamide T=60°C; 0.166667 h;
参考文献
Herbivo, Cyril; Comel, Alain; Kirsch; Raposo, M. Manuela M.
Tetrahedron, 2009 , vol. 65, # 10 p. 2079 - 2086
反应条件
1: β-chloro cinnamaldehyde With Na2S*9H2O in N,N-dimethyl-formamide T=60°C; 2 h; 2: monochloroacetaldehyde in N,N-dimethyl-formamide T=60°C; 3 h; 3: With potassium carbonate in water; N,N-dimethyl-formamide T=60°C; 0.166667 h;
参考文献
Herbivo, Cyril; Comel, Alain; Kirsch; Fonseca, A. Mauricio C.; Belsley, M.; Raposo, M. Manuela M.
Dyes and Pigments, 2010 , vol. 86, # 3 p. 217 - 226
反应条件
1: 99.5 percent / ethanolic HCl / 2 h / Ambient temperature 2: 48 percent / 0.05 h / 220 - 250 °C View Scheme
参考文献
Roy; Kar; Ray
Synthetic Communications, 1993 , vol. 23, # 14 p. 1959 - 1965
反应条件
potassium carbonate in acetonitrile 0.0833333 h; microwave irradiation;
参考文献
Heterocyclic Communications, , vol. 10, # 6 p. 411 - 414
反应条件
1,4-diaza-bicyclo[2.2.2]octane; AlCl3, aluminium chloride T=20°C; Baylis-Hillman reaction; 10 h; Neat (no solvent);
参考文献
Zhong, Weihui; Chen, Yanhui; Wang, Guan
Journal of Chemical Research, 2010 , # 1 p. 44 - 49
