(1-溴-1-丙烯-2-基)苯合成路线 （共 15 条）
反应条件
N-bromosuccinmide; meta-chloroperoxybenzoic acid
参考文献
Wyrick, Steven D.; Booth, Raymond G.; Myers, Andrew M.; Owens, Constance E.; Bucholtz, Ehren C.; et al.
Journal of Medicinal Chemistry, 1995 , vol. 38, # 19 p. 3857 - 3864
反应条件
N-bromosuccinmide; anhydrous lithium acetate in water; acetonitrile 1 h;
参考文献
Chowdhury, Shantanu; Roy, Sujit
Journal of Organic Chemistry, 1997 , vol. 62, # 1 p. 199 - 200
反应条件
N-bromosuccinmide; tetrabutyl-ammonium trifluoroacetate in 1,2-dichloro-ethane T=20°C; Decarboxylation; bromination; Hunsdiecker reaction; 4 h;
参考文献
Naskar, Dinabandhu; Roy, Sujit
Tetrahedron, 2000 , vol. 56, # 10 p. 1369 - 1377
反应条件
1: With bromine in tetrachloromethane 18 h; 2: With potassium hydroxide; 18-crown-6 ether in hexane 36 h; Heating; Further stages.;
参考文献
Annunziata, Alfonso; Galli, Carlo; Gentili, Patrizia; Guarnieri, Alessandra; Beit-Yannai, Michal; Rappoport, Zvi
European Journal of Organic Chemistry, 2002 , # 13 p. 2136 - 2143
反应条件
n-butyllithium in tetrahydrofuran; diethyl ether; Petroleum ether T=-100°C;
参考文献
Entmayr,P.; Koebrich,G.
Chemische Berichte, 1976 , vol. 109, p. 2175 - 2184
反应条件
1: isopropenylbenzene With N-bromosuccinmide in tetrachloromethane T=95 - 100°C; 10 h; 2: With triphenylphosphine in benzene 3: benzaldehyde With n-butyllithium in tetrahydrofuran; hexane T=20°C; 1.5 h;
参考文献
Lambert, Joseph B.; Liu, Chunqing; Kouliev, Timur
Journal of Physical Organic Chemistry, 2002 , vol. 15, # 9 p. 667 - 671
反应条件
1: (i) iPr2NLi, (ii) /BRN= 605842/, (iii) /BRN= 1209232/ 2: nBuLi / tetrahydrofuran; diethyl ether; petroleum ether / -100 °C View Scheme
参考文献
Entmayr,P.; Koebrich,G.
Chemische Berichte, 1976 , vol. 109, p. 2175 - 2184
反应条件
piperidine; tert.-butyl lithium 1) ether, pentane, 2) ether, pentane, reflux, 30 min; Multistep reaction;
参考文献
Axelrad, George; Laosooksathit, Surin; Engel, Robert
Journal of Organic Chemistry, 1981 , vol. 46, p. 5200 - 5204
反应条件
(tBuOOCO)2; hydrogen bromide; oxygen in tetrahydrofuran; hexane T=30°C; 1 h; pH=2-4; Product distribution;
参考文献
Jiang, Xi-Kui; Liu, Wayne Wei-Zhong; Wu, Shi-Hui
Journal of Physical Organic Chemistry, 1994 , vol. 7, p. 96 - 104
反应条件
T=350°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Jiang, Xi-Kui; Liu, Wayne Wei-Zhong; Wu, Shi-Hui
Journal of Physical Organic Chemistry, 1994 , vol. 7, p. 96 - 104
