三甲基硅基三甲硅氧基醋酸酯合成路线 （共 12 条）
反应条件
pyridine in acetonitrile 1 h; Product distribution / selectivity;
参考文献
Florida State University Research Foundation, Inc.
Patent: US2006/281914 A1, 2006 ;
Location in patent: Page/Page column 10 ;
反应条件
in acetonitrile T=60°C;
参考文献
Journal of the American Chemical Society, , vol. 109, # 9 p. 2836 - 2837
反应条件
in hexane; dichloromethane T=60°C; Substitution; 0.666667 h;
参考文献
Environmental Science and Technology, , vol. 32, # 16 p. 2357 - 2370
反应条件
pyridine; ammonium sulfate
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 42, p. 1165 - 1169
反应条件
trimethylsilylating agent multistep reaction: 1.) 125 deg C, 6 h, 2.) trimethylsilylation; further temperature, time effect; Product distribution;
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 34, # 9 p. 633 - 636
反应条件
trimethylsilyl iodide in dichloromethane T=-78°C; 3 h;
参考文献
Pearson, William H.; Cheng, Minn-Chang
Journal of Organic Chemistry, 1987 , vol. 52, # 7 p. 1353 - 1355
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane T=-78°C; 4 h;
参考文献
Pearson, William H.; Cheng, Minn-Chang
Journal of Organic Chemistry, 1987 , vol. 52, # 7 p. 1353 - 1355
反应条件
pyridine; trimethylsilyl trifluoromethanesulfonate 1) -40 deg C, 30 min, 2) up to 10 deg C, 4 h;
参考文献
Schwenker; Stiefvater
Archiv der Pharmazie, 1991 , vol. 324, # 5 p. 307 - 311
反应条件
lithium chloride in tetrahydrofuran; hexane
参考文献
American Cyanamid Company
Patent: US4297516 A1, 1981 ;
反应条件
triethylamine 14 h; Ambient temperature;
参考文献
Oesterle, Thomas; Simchen, Gerhard
Liebigs Annalen der Chemie, 1987 , p. 687 - 692
