2-环己烯-1-基苯甲酸酯合成路线 （共 25 条）
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in benzene T=80°C; 8 h;
参考文献
Shi, Erbo; Shao, Ying; Chen, Shulin; Hu, Huayou; Liu, Zhaojun; Zhang, Jie; Wan, Xiaobing
Organic Letters, 2012 , vol. 14, # 13 p. 3384 - 3387
反应条件
pyridine in dichloromethane 17 h; Ambient temperature;
参考文献
Mowery, Molly E.; DeShong, Philip
Journal of Organic Chemistry, 1999 , vol. 64, # 2-5 p. 1684 - 1688
反应条件
chiral 1,10-phenanthroline; copper(II) bis(trifluoromethanesulfonate); phenylhydrazine in acetone T=20°C; 0.5 h;
参考文献
Chelucci, Giorgio; Loriga, Giovanni; Murineddu, Gabriele; Pinna, Gerard A
Tetrahedron Letters, 2002 , vol. 43, # 19 p. 3601 - 3604
反应条件
in tetrahydrofuran; toluene T=-45°C; Inert atmosphere;
参考文献
Wommack, Andrew J.; Moebius, David C.; Travis, Austin L.; Kingsbury, Jason S.
Organic Letters, 2009 , vol. 11, # 15 p. 3202 - 3205
反应条件
tert.-butylhydroperoxide; copper diacetate in decane T=140°C; 24 h; Schlenk techniqueInert atmosphere; Reagent/catalystTemperatureConcentration;
参考文献
Zhao, Jincan; Fang, Hong; Han, Jianlin; Pan, Yi
Organic Letters, 2014 , vol. 16, # 9 p. 2530 - 2533
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene T=20°C; 24 h;
参考文献
Utsunomiya, Masaru; Kawatsura, Motoi; Hartwig, John F.
Angewandte Chemie - International Edition, 2003 , vol. 42, # 47 p. 5865 - 5868
反应条件
4-(N,N-dimethlyamino)pyridine; pivaloyl chloride in dichloromethane T=100°C; Microwave irradiation;
参考文献
Gill, Monica A.; Manthorpe, Jeffrey M.
Synthetic Communications, 2013 , vol. 43, # 10 p. 1460 - 1468
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene T=120°C; 3 h;
参考文献
Gupta, Ajay K.; Kazlauskas, Romas J.
Tetrahedron: Asymmetry, 1993 , vol. 4, # 5 p. 879 - 888
反应条件
Grubb's 2nd generation catalyst in ethyl acetate T=20°C;
参考文献
Scholte, Andrew A.; Mi, Hyun An; Snapper, Marc L.
Organic Letters, 2006 , vol. 8, # 21 p. 4759 - 4762
反应条件
1: 1.) LDA, 2.) TMSCl, 4.) aq. HCl 2: 99 percent / CeCl3*H2O, NaBH4 / methanol / 0.17 h 3: 93 percent / DMAP / CH2Cl2 / 24 h / Heating 4: tributyltin hydride, AIBN / benzene / 8 h / Heating View Scheme
参考文献
Crich, David; Yao, Qingwei; Filzen, G. Fredrick
Journal of the American Chemical Society, 1995 , vol. 117, # 46 p. 11455 - 11470
