1-(2-甲氧基苯基)-2-苯乙酮合成路线 （共 21 条）
反应条件
scandium tris(trifluoromethanesulfonate) in toluene T=-78°C; 0.166667 h; Inert atmosphere;
参考文献
Wommack, Andrew J.; Moebius, David C.; Travis, Austin L.; Kingsbury, Jason S.
Organic Letters, 2009 , vol. 11, # 15 p. 3202 - 3205
反应条件
potassium phosphate; palladium diacetate; tri-cyclo-hexyl-phosphine in water T=80°C; Suzuki carbonylation; P=7500.75 Torr; 20 h; Inert atmosphere;
参考文献
Wu, Xiao-Feng; Neumann, Helfried; Beller, Matthias
Tetrahedron Letters, 2010 , vol. 51, # 47 p. 6146 - 6149
反应条件
toluene-4-sulfonic acid in ethanol T=170°C; microwave irradiation;
参考文献
Jacubert, Maud; Hamze, Abdallah; Provot, Olivier; Peyrat, Jean-Francois; Brion, Jean-Daniel; Alami, Mouad
Tetrahedron Letters, 2009 , vol. 50, # 26 p. 3588 - 3592
反应条件
potassium hydroxide in ethanol; water Heating;
参考文献
McEwen, William E.; Grossi, Anthony V.; MacDonald, Russell J.; Stamegna, Andrew P.
Journal of Organic Chemistry, 1980 , vol. 45, # 7 p. 1301 - 1308
反应条件
1: 1-iodo-2-methoxybenzene With magnesium in diethyl ether T=20°C; Metallation; 1 h; 2: With cadmium (II) chloride in diethyl ether T=20°C; Metallation; 1 h; 3: phenylacetyl chloride in benzene T=0°C; Substitution; Heating;
参考文献
Ghosh, Somnath; Banerjee, Indira; Baul, Susmita
Tetrahedron, 1999 , vol. 55, # 38 p. 11537 - 11546
反应条件
tris-(dibenzylideneacetone)dipalladium(0); bis[2-(diphenylphosphino)phenyl] ether; sodium t-butanolate in tetrahydrofuran T=70°C; Schlenk techniqueInert atmosphere;
参考文献
Mehta, Vaibhav P.; Garcia-Lopez, Jose-Antonio; Greaney, Michael F.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 6 p. 1529 - 1533
Angew. Chem., 2014 , vol. 126, # 6 p. 1555 - 1559,5
反应条件
NiBr2bipy; tetra-n-butylammonium tetrafluoroborate in N,N-dimethyl-formamide Electrochemical reaction;
参考文献
Dolhem, Eric; Barhdadi, Rachid; Folest, Jean Claude; Nedelec, Jean Yves; Troupel, Michel
Tetrahedron, 2001 , vol. 57, # 3 p. 525 - 529
反应条件
diethyl ether anschliessend mit wss. HCl;
参考文献
Otter; Shriner
Journal of the American Chemical Society, 1951 , vol. 73, p. 887,888
反应条件
1: 94 percent / pyridine / Ambient temperature 2: 80 percent / NaH / dimethylformamide 3: 94 percent / KOH / ethanol; H2O / Heating View Scheme
参考文献
McEwen, William E.; Grossi, Anthony V.; MacDonald, Russell J.; Stamegna, Andrew P.
Journal of Organic Chemistry, 1980 , vol. 45, # 7 p. 1301 - 1308
反应条件
2: 94 percent / pyridine / Ambient temperature 3: 80 percent / NaH / dimethylformamide 4: 94 percent / KOH / ethanol; H2O / Heating View Scheme
参考文献
McEwen, William E.; Grossi, Anthony V.; MacDonald, Russell J.; Stamegna, Andrew P.
Journal of Organic Chemistry, 1980 , vol. 45, # 7 p. 1301 - 1308
