1: With diisobutylaluminium hydride in tetrahydrofuran; hexane T=-78 - 20°C; 19 h; 2: With hydrogenchloride in tetrahydrofuran; hexane; water T=0°C;
参考文献
Mathias, John Paul; Millan, David Simon; Lewthwaite, Russell Andrew; Phillips, Christopher
Patent: US2006/35922 A1, 2006 ;
Location in patent: Page/Page column 31 ;
US 20060035922 A1
1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 3 h / -78 - 20 °C
2: caesium carbonate / acetonitrile / 2 h / 20 °C
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参考文献
LG LIFE SCIENCES LTD.; KIM, Young Kwan; KIM, Myoung Yeol; PARK, Sang Yun; PARK, Ok Ku; ARTEMOV, Vasily; LEE, Sang Dae; JOO, Hyun Woo; CHOI, Eun Sil
Patent: WO2014/69963 A1, 2014 ;