2-哌啶-1-基环己烷-1-酮合成路线 （共 7 条）
反应条件
oxalyl dichloride; triethylamine in dichloromethane; dimethyl sulfoxide T=20°C; Swern oxidation; 2.5 h;
参考文献
Liu, Sheng; Xie, Jian-Hua; Wang, Li-Xin; Zhou, Qi-Lin
Angewandte Chemie - International Edition, 2007 , vol. 46, # 39 p. 7506 - 7508
反应条件
MoVIO2(acetylacetone)2; alpha,alpha-dimethylbenzyl hydroperoxide T=20 - 30°C; 1 h;
参考文献
Blau, Karla; Voerckel, V.
Journal fuer Praktische Chemie (Leipzig), 1989 , vol. 331, # 2 p. 285 - 292
参考文献
Blau, Karla; Voerckel, V.
Journal fuer Praktische Chemie (Leipzig), 1989 , vol. 331, # 2 p. 285 - 292
反应条件
in benzene 72 h; Heating; Yield given. Yields of byproduct given;
参考文献
Fraenkel, Gideon; Gallucci, Judith; Rosenzweig, Howard S.
Journal of Organic Chemistry, 1989 , vol. 54, # 3 p. 677 - 681
反应条件
1: 68 percent / 4 h 2: 35 percent / Cumene hydroperoxide, MoO2(acac)2 / 1 h / 20 - 30 °C View Scheme
参考文献
Blau, Karla; Voerckel, V.
Journal fuer Praktische Chemie (Leipzig), 1989 , vol. 331, # 2 p. 285 - 292
反应条件
1: 68 percent / 4 h 2: 35 percent / Cumene hydroperoxide, MoO2(acac)2 / 1 h / 20 - 30 °C View Scheme
参考文献
Blau, Karla; Voerckel, V.
Journal fuer Praktische Chemie (Leipzig), 1989 , vol. 331, # 2 p. 285 - 292
反应条件
oxygen T=20°C; further temperature: 50 deg C, reaction also with the solvents: chloroform, benzene, diethyl ether; Product distribution;
参考文献
Blau, Karla; Voerckel, V.
Journal fuer Praktische Chemie (Leipzig), 1989 , vol. 331, # 2 p. 285 - 292
