1-甲基-4-苯基乙炔苯合成路线 (共 165 条)
反应条件
W(CCMe3)(O=PEt2)Cl3 in tetrahydrofuran
T=60°C; estimated rate and time of equilibrium (2 h);
参考文献
Wengrovius,J.H.; Sancho,J.; Schrock,R.R.
Journal of the American Chemical Society, 1981 , vol. 103, p. 3932
反应条件
lead dioxide; trifluoroacetic acid in dichloromethane
T=0°C; 1.5 h;
参考文献
Vasil'ev; Rudenko
Russian Journal of Organic Chemistry, 2010 , vol. 46, # 9 p. 1282 - 1289
反应条件
N-bromosuccinmide; dibenzoyl peroxide
参考文献
Tashchuk,K.G.; Dombrovskii,A.V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1965 , vol. 1, p. 503 - 507
Khimiya Geterotsiklicheskikh Soedinenii, 1965 , vol. 1, # 5 p. 744 - 749
反应条件
lt;W(N(i-Pr)2)3(C-t-Bu)gt; in toluene
T=25°C; 1 h;
参考文献
Leigh, G. Jeffery; Rahman, Mohammed T.; Walton, David R. M.
Journal of the Chemical Society, Chemical Communications, 1982 , # 9 p. 541 - 542
反应条件
in decalin
A mixture of p-tolyl(phenyl)acetylene and the iron-benzoyl-d5-complex is heated in decalin to reflux and maintained at reflux for 5 min. (further products); cooling, sepn. by chromy. on an alumina column;
参考文献
Butler, Ian R.; Elliot, Joanne L.; Houde, Jean
Canadian Journal of Chemistry, 1990 , vol. 68, # 9 p. 1564 - 1573