1,1,3,3-四甲基二硅氧烷合成路线 （共 158 条）
反应条件
platinum(0)-2,4,6,8-tetramethyl-2,4,6,8-tetravinylcyclotetrasiloxane T=70 - 140°C; 1.16667 h;
参考文献
US2007/249502 A1, ;
Page/Page column 23 ;
反应条件
lithium bromide in dichloromethane; acetonitrile
参考文献
SmithKline Beecham Corporation
Patent: US5393788 A1, 1995 ;
US 5393788 A
反应条件
tris(1,3-divinyl-1,1,3,3-tetramethyldisiloxane)-bis-platinum(0) in toluene T=20°C; 4 h; Reflux;
参考文献
Frampton, Mark B.; Subczynska, Izabela; Zelisko, Paul M.
Biomacromolecules, 2010 , vol. 11, # 7 p. 1818 - 1825
反应条件
dihydrogen hexachloroplatinate in isopropyl alcohol; toluene T=100°C; 6 h; Title compound not separated from byproducts;
参考文献
Iojoiu, Cristina; Sava, Mitica; Pinteala, Mariana; Harabagiu, Valeria; Abadie, Marc J. M.; Simionescu, Bogdan C.; Simionescu, Cristofor I.
Revue Roumaine de Chimie, 2001 , vol. 46, # 7 p. 703 - 711
反应条件
hydrogenchloride in water; toluene T=47°C; 1 h; Inert atmosphere;
参考文献
MOMENTIVE PERFORMANCE MATERIALS GMBH
Patent: US2012/46485 A1, 2012 ;
Location in patent: Page/Page column 5 ;
参考文献
Russian Journal of General Chemistry, , vol. 73, # 1 p. 157 - 157
反应条件
1: methanol With 5 palladium on charcoal in water T=50°C; Reflux; 2: 1,1,3,3-tetramethyldisiloxane T=50°C; 2.75 h; Product distribution / selectivity;
参考文献
WACKER CHEMIE AG
Patent: US2012/10422 A1, 2012 ;
Location in patent: Page/Page column 6 ;
反应条件
22 h; Ambient temperature;
参考文献
Drake, John E.; Glavincevski, Boris M.; Hemmings, Raymond T.
Canadian Journal of Chemistry, 1980 , vol. 58, # 20 p. 2161 - 2166
反应条件
dihydrogen hexachloroplatinate
参考文献
Saam; Speier
Journal of the American Chemical Society, 1958 , vol. 80, p. 4104
反应条件
Pd0(tris(tert-butyl)phosphine)2; N-ethyl-N,N-diisopropylamine in tetrahydrofuran T=20°C; 4 h;
参考文献
Kurihara, Yu; Yamanoi, Yoshinori; Nishihara, Hiroshi
Chemical Communications, 2013 , vol. 49, # 96 p. 11275 - 11277
