2,3,4,5-四苯基吡咯合成路线 (共 51 条)
反应条件
titanium tetrachloride; triethylamine in dichloromethane T=0 - 25°C;
参考文献
Periasamy, Mariappan; Srinivas, Gadthula; Seenivasaperumal, Muthu
Journal of Chemical Research, 2004 , # 4 p. 270 - 272
反应条件
ammonium acetate; acetic acid T=130°C; Paal-Knorr pyrrole synthesis; 24 h;
参考文献
Kuo, Wen-Jang; Chen, Ying-Hsiao; Jeng, Ru-Jong; Chan, Li-Hsin; Lin, Wen-Peng; Yang, Zhe-Ming
Tetrahedron, 2007 , vol. 63, # 30 p. 7086 - 7096
反应条件
PEG-200; ammonium formate; palladium on activated charcoal 0.116667 h; microwave irradiation;
参考文献
Rao, H. Surya Prakash; Jothilingam; Scheeren, Hans W.
Tetrahedron, 2004 , vol. 60, # 7 p. 1625 - 1630
反应条件
1: With dichlorobis(dicyclohexylphosphinomethylpyridine)–ruthenium (II); potassium tert-butylate T=165°C; 24 h; Inert atmosphere; 2: With sodium tetrahydroborate in methanol T=20°C; Inert atmosphere;
参考文献
Iida, Kazuki; Miura, Takashi; Ando, Junki; Saito, Susumu
Organic Letters, 2013 , vol. 15, # 7 p. 1436 - 1439
反应条件
titanium(III) chloride in tetrahydrofuran; water T=35°C; 24 h; pH 6.5;
参考文献
Sera, Akira; Fukumoto, Shoji; Tamura, Masako; Takabatake, Kiyoshi; Yamada, Hiroaki; Itoh, Kuniaki
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 6 p. 1787 - 1791
反应条件
titanium(III) chloride; ammonium acetate in tetrahydrofuran; water T=35°C; 24 h;
参考文献
Sera, Akira; Fukumoto, Shoji; Yoneda, Takako; Yamada, Hiroaki
Heterocycles, 1986 , vol. 24, # 3 p. 697 - 702
反应条件
sodium hydrogensulfite; copper(I) bromide in dimethyl sulfoxide T=140°C; 2 h; Inert atmosphere;
参考文献
Ran, Longfei; Ren, Zhi-Hui; Wang, Yao-Yu; Guan, Zheng-Hui
Green Chemistry, 2014 , vol. 16, # 1 p. 112 - 115
反应条件
1: 72 percent / diethyl ether / 2 h / 0 °C 2: thioxanthen-9-one / benzene / Irradiation View Scheme
参考文献
Zimmerman, Howard E.; Wright, Charles W.
Journal of the American Chemical Society, 1992 , vol. 114, # 1 p. 363 - 365
反应条件
1: 72 percent / diethyl ether / 2 h / 0 °C 2: thioxanthen-9-one / benzene / Irradiation View Scheme
参考文献
Zimmerman, Howard E.; Wright, Charles W.
Journal of the American Chemical Society, 1992 , vol. 114, # 1 p. 363 - 365
反应条件
in benzene T=80°C; 3 h;
参考文献
Hong, Pangbu; Yamazaki, Hiroshi
Journal of Organometallic Chemistry, 1989 , vol. 373, p. 133 - 142