3,3,4,4-四氯联苯合成路线 （共 22 条）
反应条件
potassium phosphate; palladium diacetate in water; N,N-dimethyl-formamide T=20°C; Inert atmosphere;
参考文献
Akzinnay, Said; Bisaro, Fabrice; Cazin, Catherine S. J.
Chemical Communications, 2009 , # 38 p. 5752 - 5753
反应条件
1: With n-butyllithium in tetrahydrofuran; hexanes T=-78°C; 1 h; Inert atmosphere; 2: With copper(ll) bromide in tetrahydrofuran; hexanes T=-78°C; 3 h; Inert atmosphere;
参考文献
Er, Joyce A. V.; Tennyson, Andrew G.; Kamplain, Justin W.; Lynch, Vincent M.; Bielawski, Christopher W.
European Journal of Inorganic Chemistry, 2009 , # 13 SPEC. ISS. p. 1729 - 1738
反应条件
tetracarbonylbis(μ-chloro)dirhodium(I); di-tert-butyl peroxide; triphenylphosphine in benzene T=150°C; 12 h; Inert atmosphere; chemoselective reaction;
参考文献
Yang, Luo; Zeng, Tieqiang; Shuai, Qi; Guo, Xiangyu; Li, Chao-Jun
Chemical Communications, 2011 , vol. 47, # 7 p. 2161 - 2163
反应条件
titanium(IV) isopropylate; bis(benzonitrile)palladium(II) dichloride in m-xylene T=140°C; 2 h;
参考文献
Miura, Masahiro; Hashimoto, Hideo; Itoh, Kenji; Nomura, Masakatsu
Chemistry Letters, 1990 , # 3 p. 459 - 460
反应条件
sodium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane; ethanol Heating;
参考文献
Kania-Korwel, Izabela; Parkin, Sean; Robertson, Larry W.; Lehmler, Hans-Joachim
Chemosphere, 2004 , vol. 56, # 8 p. 735 - 744
反应条件
ceric pyridinium nitrate; mercury(II) diacetate T=110°C; Condensation; 24 h;
参考文献
Iranpoor, Nasser; Shekarriz, Marzieh
Journal of Chemical Research - Part S, 1999 , # 7 p. 442 - 443
反应条件
palladium diacetate in N,N-dimethyl-formamide
参考文献
Phillipson; Puma
Analytical Chemistry, 1980 , vol. 52, # 14 p. 2328 - 2332
反应条件
sulfuric acid Diazotization.Behandlung der Diazoniumsalz-Loesung mit CuCl in wss. HCl;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 53, p. 359,362
参考文献
Acta Chemica Scandinavica (1947-1973), , vol. 27, p. 600 - 604
反应条件
palladium diacetate; N-ethyl-N,N-diisopropylamine; triphenylphosphine in water; toluene T=70°C; Suzuki-Miyaura coupling; 1.08333 h; KineticsMechanism; ConcentrationTemperatureTime;
参考文献
Organic Process Research and Development, , vol. 13, # 3 p. 420 - 428
