4,4’-二氰基二苯甲酮合成路线 (共 11 条)
反应条件
sodium carbonate; palladium dichloride in N,N-dimethyl acetamide T=25 - 100°C; 6 h;
参考文献
US2007/100149 A1, ;
Page/Page column 6 ;
反应条件
1: carbon monoxide With 1,1'-bis-(diphenylphosphino)ferrocene; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in tetrahydrofuran T=20°C; P=760.051 Torr; 0.166667 h; 2: (4-cyanophenyl)zinc(II) iodide With ethylene dibromide in tetrahydrofuran T=60°C; 3 h;
参考文献
Kobayashi, Kana; Nishimura, Yugo; Gao, Fuxing; Gotoh, Kazuma; Nishihara, Yasushi; Takagi, Kentaro
Journal of Organic Chemistry, 2011 , vol. 76, # 6 p. 1949 - 1952
反应条件
CuCN in ethyl acetate; N,N-dimethyl-formamide
反应条件
2,3-dimethyl-naphthalene in acetonitrile 0.00277778 h; microwave irradiation;
参考文献
Enquist, Per-Anders; Nilsson, Peter; Larhed, Mats
Organic Letters, 2003 , vol. 5, # 25 p. 4875 - 4878
反应条件
bis(1,5-cyclooctadiene)nickel (0) in N,N-dimethyl-formamide T=50°C; 4 h;
参考文献
Goto, Toshio; Onaka, Makoto; Mukaiyama, Teruaki
Chemistry Letters, 1980 , p. 51 - 52
反应条件
3-chloroprop-1-ene; cobalt(II) dibromide; zinc; trifluoroacetic acid in acetonitrile 2 h;
参考文献
Journal of Organic Chemistry, , vol. 69, # 3 p. 936 - 942
反应条件
2,3,11,12-dicyclohexano-1,4,7,10,13,16-hexaoxacyclo-octadecane; potassium permanganate in benzene
参考文献
Journal of the American Chemical Society, , vol. 96, # 24 p. 7445 - 7453
反应条件
in N,N-dimethyl-formamide T=140°C; 24 h;
参考文献
Tomioka, Hideo; Yamamoto, Katsutoshi
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 1 p. 63 - 66
反应条件
hydrogenchloride; water; sodium nitrite weiteres Reagens: Natriumcarbonat;
参考文献
Journal of the Chemical Society, , p. 103,107
反应条件
sulfuric acid Heating;
参考文献
Tomioka, Hideo; Yamamoto, Katsutoshi
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 1 p. 63 - 66