2-甲基-3-戊基环氧乙烷合成路线 （共 32 条）
反应条件
1: alcoholic KOH-solution 2: acid 3: potassium hydroxide; anhydrous diethyl ether View Scheme
参考文献
Detoeuf
Bulletin de la Societe Chimique de France, 1922 , vol. <4> 31, p. 178
反应条件
chloro-trimethyl-silane; zinc in dichloromethane 0.0833333 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Vankar, Yashwant D.; Arya, Padmashree S.; Rao, C. Trinadha
Synthetic Communications, 1983 , vol. 13, # 10 p. 869 - 872
参考文献
Kirrmann; Chancel
Bulletin de la Societe Chimique de France, 1951 , p. 227
反应条件
chloro-trimethyl-silane; zinc in dichloromethane 0.0833333 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Vankar, Yashwant D.; Arya, Padmashree S.; Rao, C. Trinadha
Synthetic Communications, 1983 , vol. 13, # 10 p. 869 - 872
反应条件
sodium tetrahydroborate; bis(tetra-n-butylammonium) tetrakis(benzenethiolato-.mu.3-sulphido-iron) in ethanol; acetonitrile T=25°C; 3 h;
参考文献
Itoh, Takashi; Nagano, Tetsuo; Sato, Mitsuo; Hirobe, Masaaki
Tetrahedron Letters, 1989 , vol. 30, # 46 p. 6387 - 6388
反应条件
bis(cyclopentadienyl)titanium dichloride; magnesium in tetrahydrofuran 12 h; Ambient temperature;
参考文献
Schobert, Rainer
Angewandte Chemie, 1988 , vol. 100, # 6 p. 869 - 871
反应条件
isopropyl alcohol in toluene T=110°C; 12 h; Inert atmosphere;
参考文献
Schobert, Rainer
Angewandte Chemie, 1988 , vol. 100, # 6 p. 869 - 871
反应条件
sodium hydrogencarbonate 1.) chloroform, 20 grad C, 24 h; Multistep reaction. Yields of byproduct given;
参考文献
Cravador, A.; Krief, A.
Tetrahedron Letters, 1981 , vol. 22, # 26 p. 2491 - 2494
反应条件
Tris(methylseleno)borane; sodium hydrogencarbonate 1.) chloroform, 20 grad C, 24 h; Multistep reaction;
参考文献
Cravador, A.; Krief, A.
Tetrahedron Letters, 1981 , vol. 22, # 26 p. 2491 - 2494
反应条件
isopropyl alcohol in toluene
T=110°C; 12 h; Inert atmosphere;
参考文献
Schobert, Rainer
Angewandte Chemie, 1988 , vol. 100, # 6 p. 869 - 871
