3-甲基-1-戊烯-4-炔-3-醇合成路线 （共 33 条）
反应条件
sulfuric acid; sodium in diethyl ether; ammonia; water
参考文献
Hoffmann-La Roche Inc.
Patent: US3950446 A1, 1976 ;
反应条件
sulfuric acid; sodium; magnesium in diethyl ether; ammonia; water
参考文献
Hoffmann-La Roche Inc.
Patent: US3950446 A1, 1976 ;
反应条件
sodium hydroxide in methanol; water T=40°C; 0.75 h;
参考文献
Bychkova, N. A.; Zotchik, N. V.; Motorina, Zh. N.; Rubtsov, I. A.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 5 p. 1111 - 1117,990 - 995
反应条件
1: With 4,4'-di-tert-butylbiphenyl in tetrahydrofuran T=-10 - 0°C; 2 h; 2: With water in tetrahydrofuran T=20°C;
参考文献
BASF AKTIENGESELLSCHAFT
Patent: WO2004/18399 A1, 2004 ;
Location in patent: Page/Page column 5-6 ;
反应条件
sulfuric acid in diethyl ether; water
反应条件
hydrogen; palladium in ethanol T=29.9°C; P=15001.2 Torr; different catalysts (group VIII);
参考文献
Russian Journal of Physical Chemistry, , vol. 64, # 1 p. 43 - 46
Zhurnal Fizicheskoi Khimii, , vol. 64, # 1 p. 83 - 87
反应条件
acetylene in tetrahydrofuran T=35°C; 2.75 h;
参考文献
Journal of Organic Chemistry, , vol. 29, p. 1872 - 1876
参考文献
Jung, Michael E.; Duclos, Brian A.
Tetrahedron Letters, 2004 , vol. 45, # 1 p. 107 - 109
参考文献
Gabriele; Salerno; Lauria
Journal of Organic Chemistry, 1999 , vol. 64, # 21 p. 7687 - 7692
反应条件
sulfuric acid; hydroquinone; mercury dichloride in di-isopropyl ether T=50 - 52°C; 0.166667 h; Product distribution;
参考文献
Zacharias; Pushpakumari; Sreevalsan; Pillai
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 1 p. 59 - 62
