2-(苯基亚甲基氨基)苯酚合成路线 (共 9 条)
反应条件
magnesium sulfate in tetrahydrofuran T=20°C; Inert atmosphereGreen chemistry; Solvent;
参考文献
Shih, Yachen; Ke, Chengyi; Pan, Chinghao; Huang, Yungtzung
RSC Advances, 2013 , vol. 3, # 20 p. 7330 - 7336
反应条件
copper (II) acetate monohydrate in tetrahydrofuran T=66°C; 20 h; TemperatureReagent/catalystSolvent;
参考文献
Chen, Guo-Feng; Shen, Hai-Dong; Zhang, Li-Yan; Li, Hong-Yang; Lan, Rui-Jia; Chen, Bao-Hua; Li, Ji-Tai; Hu, Qing-Hui
Letters in Organic Chemistry, 2014 , vol. 11, # 3 p. 180 - 187
反应条件
1: o-hydroxynitrobenzene With chromium dichloride; manganese; chloro-trimethyl-silane in N,N-dimethyl-formamide T=20°C; 0.25 h; 2: benzaldehyde in N,N-dimethyl-formamide T=20°C; 18 h;
参考文献
Hari; Karan; Rodrigues; Miller
Journal of Organic Chemistry, 2001 , vol. 66, # 3 p. 991 - 996
参考文献
Poroiskaya, S. M.; Kharitonov, G. V.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 4 p. 933 - 936,756 - 758
反应条件
2,6-di-tert-butyl-4-methylpyridine; thianthrene cation radical perchlorate in acetonitrile 0.0833333 h; Ambient temperature;
参考文献
Park, Koon Ha; Jun, Kun; Shin, Seung Rim; Oh, Sea Wha
Tetrahedron Letters, 1996 , vol. 37, # 49 p. 8869 - 8870
反应条件
degassed in 2-methyl cyclohexane Ambient temperatureIrradiationother reagent: O2; var. N-arylidene-o-aminophenols; Product distribution;
参考文献
Tauer, Erich; Grellmann, Karl H.
Journal of Organic Chemistry, 1981 , vol. 46, # 21 p. 4252 - 4258
反应条件
1: (S)-6,6'-dibromo-1,1'-bi-2-naphthol-1,2-dimethylimidazole - Zr(IV) complex / toluene / -78 °C 2: K2CO3 3: cerium ammonium nitrate / methanol 4: 100 percent / 10percent aq. HCl / Heating View Scheme
参考文献
Kobayashi; Ishitani; Ueno
Journal of the American Chemical Society, 1998 , vol. 120, # 2 p. 431 - 432
反应条件
dirhodium tetraacetate in dichloromethane Heating;
参考文献
Huang, Haoxi; Guo, Xin; Hu, Wenhao
Angewandte Chemie - International Edition, 2007 , vol. 46, # 8 p. 1337 - 1339
反应条件
1.1: diisopropyl (R,R)-tartrate; butylmagnesium bromide; Et2Zn / CH2Cl2; tetrahydrofuran; hexane / 0 °C
1.2: H2O / CH2Cl2; tetrahydrofuran / 0 °C
1.3: CH2Cl2 / 0 °C
2.1: MeI; Na2CO3
2.2: CAN
View Scheme
参考文献
Ukaji, Yutaka; Takenaka, Shoichi; Horita, Yoshie; Inomata, Katsuhiko
Chemistry Letters, 2001 , # 3 p. 254 - 255