2-氯-4-硫代氰酰基苯胺合成路线 （共 6 条）
反应条件
poly[4-diacetoxyiodo]styrene in acetonitrile T=20°C; 1.5 h; regioselective reaction;
参考文献
Wu, Liqiang; Chao, Shujun; Wang, Xiao; Yan, Fulin
Phosphorus, Sulfur and Silicon and the Related Elements, 2011 , vol. 186, # 2 p. 304 - 310
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in methanol T=20°C; 0.833333 h;
参考文献
Memarian, Hamid R.; Mohammadpoor-Baltork, Iraj; Nikoofar, Kobra
Canadian Journal of Chemistry, 2007 , vol. 85, # 11 p. 930 - 937
反应条件
silica-gel-supported sulfuric acid; urea hydrogen peroxide addition compound in water 0.583333 h; regioselective reaction;
参考文献
Zolfigol, Mohammad Ali; Khazaei, Ardeshir; Mokhlesi, Mohammad; Vahedi, Hoshang; Sajadifar, Sami; Pirveysian, Mahtab
Phosphorus, Sulfur and Silicon and the Related Elements, 2012 , vol. 187, # 3 p. 295 - 304
反应条件
1: in methanol T=0°C; 2: With bromine; sodium bromide in methanol T=0 - 20°C;
参考文献
Moseley, Jonathan D.; Brown, David; Firkin, Catherine R.; Jenkin, Shelley L.; Patel, Bharti; Snape, Evan W.
Organic Process Research and Development, 2008 , vol. 12, # 6 p. 1044 - 1059
反应条件
hydrogenchloride in methanol 1 h; Heating;
参考文献
Agricultural and Biological Chemistry, , vol. 45, # 10 p. 2253 - 2258
反应条件
1.1: triethylamine / dichloromethane 2.1: Na2S*9H2O / water 2.2: 150 °C 3.1: acetic acid; dihydrogen peroxide / 3 h / 90 °C View Scheme
参考文献
Moseley, Jonathan D.; Brown, David; Firkin, Catherine R.; Jenkin, Shelley L.; Patel, Bharti; Snape, Evan W.
Organic Process Research and Development, 2008 , vol. 12, # 6 p. 1044 - 1059
