3-苯基-3-丁烯-2-酮合成路线 （共 45 条）
反应条件
morpholine; acetic acid in water 8 h; Heating;
参考文献
Rodrigues, J. Augusto R.; Siqueira-Filho, Ezequias P.; De Mancilha, Moacir; Moran, Paulo J. S.
Synthetic Communications, 2003 , vol. 33, # 2 p. 331 - 340
反应条件
tetrakis(triphenylphosphine) palladium(0); triethylamine in N,N-dimethyl-formamide T=70°C; 24 h;
参考文献
Tamura, Rui; Kato, Masami; Saegusa, Koji; Oda, Daihei; Egawa, Takafumi; Yamamoto, Tamotsu
Journal of Organic Chemistry, 1987 , vol. 52, # 8 p. 1640 - 1642
反应条件
1: With 2,6-dimethylpyridine; titanium tetrachloride in dichloromethane T=-45°C; 2: With hydrogenchloride in dichloromethane T=20°C;
参考文献
Kummer, David A.; Brenneman, Jehrod B.; Martin, Stephen F.
Synlett, 2004 , # 8 p. 1431 - 1433
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran 2 h; Ambient temperature;
参考文献
Najera, Carmen; Sansano, Jose Miguel
Tetrahedron, 1990 , vol. 46, # 11 p. 3993 - 4002
反应条件
sulfuric acid; silica gel in water; dimethyl sulfoxide 24 h; Ambient temperature;
参考文献
Pellet, Michele; Huet, Francois
Tetrahedron, 1988 , vol. 44, # 14 p. 4463 - 4468
反应条件
1: With palladium diacetate; 1,3-bis-(diphenylphosphino)propane; potassium carbonate in water; dimethyl sulfoxide T=80°C; Sonogashira coupling; 40 h; 2: With hydrogenchloride in dimethyl sulfoxide T=20°C; 0.5 h;
参考文献
Vallin; Larhed; Hallberg
Journal of Organic Chemistry, 2001 , vol. 66, # 12 p. 4340 - 4343
反应条件
sulfuric acid; silica gel in water; dimethyl sulfoxide 24 h; Ambient temperature;
参考文献
Pellet, Michele; Huet, Francois
Tetrahedron, 1988 , vol. 44, # 14 p. 4463 - 4468
反应条件
1,4-diaza-bicyclo[2.2.2]octane in 1,4-dioxane 24 h; Heating;
参考文献
Dommroese, Anne-Marie; Gruetzmacher, Hans-Friedrich
Organic Mass Spectrometry, 1987 , vol. 22, p. 437 - 443
反应条件
chloromethyl iodide in dimethyl sulfoxide 3 h; Ambient temperature; Yields of byproduct given;
参考文献
Miyano, Sotaro; Hokari, Hiroshi; Hashimoto, Harukichi
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 2 p. 534 - 539
反应条件
1: 95 percent / Br2 / AlCl3 / diethyl ether 2: 48 percent / DABCO / dioxane / 24 h / Heating View Scheme
参考文献
Dommroese, Anne-Marie; Gruetzmacher, Hans-Friedrich
Organic Mass Spectrometry, 1987 , vol. 22, p. 437 - 443
