(±)-4-溴苯乙烯环氧化物合成路线 (共 33 条)
反应条件
Hydrogenation; Product distribution;
参考文献
Park; Fuchs
Journal of Organic Chemistry, 1957 , vol. 22, p. 93
反应条件
1: With sodium hexamethyldisilazane in tetrahydrofuran T=0 - 25°C; 14 h; 2: With water in tetrahydrofuran T=25°C; 5 h; regioselective reaction;
参考文献
Murugan, Andiappan; Kadambar, Vasantha Krishna; Bachu, Sreekanth; Rajashekher Reddy; Torlikonda, Venkatarao; Manjunatha, Sulur G.; Ramasubramanian, Sridharan; Nambiar, Sudhir; Howell, Gareth P.; Withnall, Jane
Tetrahedron Letters, 2012 , vol. 53, # 43 p. 5739 - 5741
反应条件
diphosphorous tetraiodide; tetraethylammonium bromide; water in dichloromethane T=20°C; 6 h; regioselective reaction;
参考文献
Telvekar, Vikas N.; Rane, Rajesh A.
Synthetic Communications, 2010 , vol. 40, # 14 p. 2108 - 2112
反应条件
sodium tetrahydroborate in methanol; tert-butyl alcohol Yield given. Yields of byproduct given;
参考文献
Ookawa, Atsuhiro; Hiratsuka, Hiroshi; Soai, Kenso
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, p. 1813 - 1818
反应条件
Product distribution;
参考文献
Fuchs; VanderWerf
Journal of the American Chemical Society, 1954 , vol. 76, p. 1631,1634
反应条件
Hydrogenation; Product distribution;
参考文献
Park; Fuchs
Journal of Organic Chemistry, 1957 , vol. 22, p. 93
反应条件
(S,S)-salen-CoIII-OAc; water in tetrahydrofuran T=0 - 20°C; optical yield given as percent ee;
参考文献
Cattoen, Xavier; Pericas, Miquel A.
Tetrahedron, 2009 , vol. 65, # 39 p. 8199 - 8205
反应条件
water in ethanol T=27°C; 2 h; biohydrolysis using Beauveria sulfurescens; pH 8; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Pedragosa-Moreau; Morisseau; Zylber; Archelas; Baratti; Furstoss
Journal of Organic Chemistry, 1996 , vol. 61, # 21 p. 7402 - 7407
反应条件
NH4Br in tetrahydrofuran; water T=20°C; 1 h; Electrochemical reaction;
参考文献
Huang, Jing-Mei; Lin, Zhi-Quan; Chen, Dong-Song
Organic Letters, 2012 , vol. 14, # 1 p. 22 - 25
反应条件
air; 4-nitro-benzoic acid; Jacobsen's (S,S)-(salen)Co(III) catalyst in various solvent(s)
T=20°C; 48 h;
参考文献
Bartoli, Giuseppe; Bosco, Marcella; Carlone, Armando; Locatelli, Manuela; Melchiorre, Paolo; Sambri, Letizia
Organic Letters, 2004 , vol. 6, # 22 p. 3973 - 3975