N-苄基-N-(1-苯基乙基)胺合成路线 (共 52 条)
反应条件
1.1 wt Pd/NiO; hydrogen in ethanol T=25°C; P=760.051 Torr; 10 h;
参考文献
Yang, Huimin; Cui, Xinjiang; Deng, Youquan; Shi, Feng
Synthetic Communications, 2014 , vol. 44, # 9 p. 1314 - 1322
反应条件
hydrogen; Ru((R,R)-cyP2N2)HCl in benzene-d6 T=20°C; P=2280.15 Torr; 36 h; Alkaline conditionsCooling with liquid nitrogen; Product distribution / selectivity;
参考文献
Tararov, Vitali I.; Kadyrov, Renat; Riermeier, Thomas H.; Fischer, Christine; Boerner, Armin
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 5 p. 561 - 565
反应条件
sodium tetrahydroborate; nickel dichloride in methanol T=20°C; Reductive amination; 0.25 h;
参考文献
Saxena, Ira; Borah, Ruli; Sarma, Jadab C.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 4 p. 503 - 504
反应条件
NiCuFeO(x) in anhydrous xylene 24 h; Inert atmosphereSealed tubeReflux;
参考文献
Cui, Xinjiang; Dai, Xingchao; Deng, Youquan; Shi, Feng
Chemistry - A European Journal, 2013 , vol. 19, # 11 p. 3665 - 3675
反应条件
[(C5Me5)IrI2]2 in water T=115°C; 10 h; Inert atmosphere;
参考文献
Saidi, Ourida; Blacker, A. John; Farah, Mohamed M.; Marsden, Stephen P.; Williams, Jonathan M. J.
Chemical Communications, 2010 , vol. 46, # 9 p. 1541 - 1543
反应条件
n-butyllithium; hydrogen in tetrahydrofuran; hexane
参考文献
Massachusetts Institute of Technology
Patent: US5292893 A1, 1994 ;
反应条件
[1,3-bis(diphenylphosphino) propane] dichloronickel(II); 1,1-dimethylethylmagnesium chloride in diethyl ether; hexane T=25°C; 6 h;
参考文献
Wehn, Paul M.; Du Bois
Organic Letters, 2005 , vol. 7, # 21 p. 4685 - 4688
反应条件
zinc(II) tetrahydroborate; silica gel in tetrahydrofuran 10 h; Ambient temperature;
参考文献
Ranu, Brindaban C.; Sarkar, Arunkanti; Majee, Adinath
Journal of Organic Chemistry, 1997 , vol. 62, # 6 p. 1841 - 1842
反应条件
hydrogen; [Rh(DPOE)(COD)]BF4 in methanol T=100°C; P=37503.8 Torr; 9 h; Product distribution; Further Variations:CatalystsTemperatures;
参考文献
Degussa AG
Patent: US6884887 B1, 2005 ;
Location in patent: Page/Page column 9; 15-16 ;
反应条件
sodium hydrogencarbonate; [{(η5-C5Me5)IrCl}2(μ-Cl)2] in toluene T=110°C; 17 h;
参考文献
Fujita, Ken-ichi; Enoki, Youichiro; Yamaguchi, Ryohei
Tetrahedron, 2008 , vol. 64, # 8 p. 1943 - 1954