4-邻苯二甲酰亚氨基丁腈合成路线 （共 20 条）
反应条件
in ethanol 18 h; Heating;
参考文献
Ryder; Schweiger; Glidle; Cooper
Journal of Materials Chemistry, 2000 , vol. 10, # 8 p. 1785 - 1793
反应条件
in dimethyl sulfoxide T=65°C; 2 h;
参考文献
Thiruvengadam; Gould; Aberhart; Horng Jau Lin
Journal of the American Chemical Society, 1983 , vol. 105, # 16 p. 5470 - 5476
反应条件
in chloroform; water; N,N-dimethyl-formamide
参考文献
Zhang, Wentao; Liehr, Sebastian Johannes Reinhard; Velligan, Mark Douglas; Dyatkina, Natalia B.; Botyanszki, Janos; Shi, Dong-Fang; Roberts, Christopher Don; Khorlin, Alexander; Nelson, Peter Harold; Muchowski, Joseph Martin
Patent: US2002/37856 A1, 2002 ;
反应条件
N-iodo-succinimide; trimethylsilylazide in 1,2-dichloro-ethane; acetonitrile T=20 - 70°C; 3 h;
参考文献
Okamoto, Noriko; Ishikura, Minoru; Yanada, Reiko
Organic Letters, 2013 , vol. 15, # 11 p. 2571 - 2573
反应条件
triethylsilane; palladium hydroxide - carbon in ethanol 8 h; Ambient temperature;
参考文献
Kotsuki, Hiyoshizo; Ohishi, Takeshi; Araki, Tomohiro
Tetrahedron Letters, 1997 , vol. 38, # 12 p. 2129 - 2132
反应条件
1: With diethylzinc in hexane; dichloromethane T=20°C; 18 h; Inert atmosphere; 2: With acetic anhydride in hexane; dichloromethane 4 h; Inert atmosphere;
参考文献
Maury, Julien; Mouysset, Dominique; Feray, Laurence; Marque, Sylvain R. A.; Siri, Didier; Bertrand, Michele P.
Chemistry - A European Journal, 2012 , vol. 18, # 11 p. 3241 - 3247
反应条件
1: triethylamine; palladium diacetate; triphenylphosphine; copper(l) iodide / 20 °C / |Inert atmosphere 2: N-iodo-succinimide; trimethylsilylazide / 1,2-dichloro-ethane; acetonitrile / 3 h / 20 - 70 °C View Scheme
参考文献
Okamoto, Noriko; Ishikura, Minoru; Yanada, Reiko
Organic Letters, 2013 , vol. 15, # 11 p. 2571 - 2573
反应条件
1.1: water / 4 h / 100 °C 2.1: thionyl chloride / 4 h / 75 °C / Inert atmosphere 3.1: sodium iodide / acetone / 4 h / 20 °C / Darkness 4.1: diethylzinc / hexane; dichloromethane / 18 h / 20 °C / Inert atmosphere 4.2: 4 h / Inert atmosphere View Scheme
参考文献
Maury, Julien; Mouysset, Dominique; Feray, Laurence; Marque, Sylvain R. A.; Siri, Didier; Bertrand, Michele P.
Chemistry - A European Journal, 2012 , vol. 18, # 11 p. 3241 - 3247
反应条件
1.1: sodium iodide / acetone / 4 h / 20 °C / Darkness 2.1: diethylzinc / hexane; dichloromethane / 18 h / 20 °C / Inert atmosphere 2.2: 4 h / Inert atmosphere View Scheme
参考文献
Maury, Julien; Mouysset, Dominique; Feray, Laurence; Marque, Sylvain R. A.; Siri, Didier; Bertrand, Michele P.
Chemistry - A European Journal, 2012 , vol. 18, # 11 p. 3241 - 3247
反应条件
1.1: thionyl chloride / 4 h / 75 °C / Inert atmosphere 2.1: sodium iodide / acetone / 4 h / 20 °C / Darkness 3.1: diethylzinc / hexane; dichloromethane / 18 h / 20 °C / Inert atmosphere 3.2: 4 h / Inert atmosphere View Scheme
参考文献
Maury, Julien; Mouysset, Dominique; Feray, Laurence; Marque, Sylvain R. A.; Siri, Didier; Bertrand, Michele P.
Chemistry - A European Journal, 2012 , vol. 18, # 11 p. 3241 - 3247
