2’,4’-二羟基苯己酮合成路线 (共 10 条)
反应条件
1: in hydrogen fluoride T=70 - 80°C; 10 - 15 h; Autoclave; 2: With water in hydrogen fluoride T=20°C; Product distribution / selectivity;
参考文献
Honeywell International Inc.
Patent: US2006/129002 A1, 2006 ;
Location in patent: Page/Page column 3 ;
反应条件
aluminium trichloride in nitrobenzene
参考文献
Mizobuchi, Shigeyuki; Sato, Yuko
Agricultural and Biological Chemistry, 1985 , vol. 49, # 5 p. 1327 - 1334
参考文献
Journal of the American Chemical Society, , vol. 48, p. 2209
反应条件
zinc(II) chloride T=140°C;
参考文献
DE531518 , ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 18, p. 3017
反应条件
in water; acetone; acetonitrile Sonogashira reaction; 60 h; Inert atmospherePhotolysis;
参考文献
Journal of Organic Chemistry, , vol. 77, # 15 p. 6473 - 6479
参考文献
Yakugaku Zasshi, , vol. 70, p. 463
Chem.Abstr., , p. 6169
反应条件
1: 135 °C 2: ZnCl2 View Scheme
参考文献
Yakugaku Zasshi, , vol. 70, p. 463
Chem.Abstr., , p. 6169
反应条件
1: K2CO3 / acetone / 20 h / Heating 2: NH2OH*HCl, CH3COOK / ethanol / 3 h / Heating View Scheme
参考文献
Beger, J.; Binte, H.-J.; Brunne, L.; Neumann, R.
Journal fuer Praktische Chemie/Chemiker-Zeitung, 1992 , vol. 334, # 3 p. 269 - 277
反应条件
hydrogenchloride; Zn–Hg amalgam in ethanol
参考文献
Mizobuchi, Shigeyuki; Sato, Yuko
Agricultural and Biological Chemistry, 1985 , vol. 49, # 5 p. 1327 - 1334
反应条件
1: 67 percent / zinc amalgame, hydrochloric acid / ethanol
2: 75 percent / aluminum chloride / nitrobenzene
View Scheme
参考文献
Liu, Peng; Xu, Xing; Chen, Lili; Ma, Lei; Shen, Xu; Hu, Lihong
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 5 p. 1596 - 1607