乙基3,4,5-三乙氧基苯甲酸酯合成路线 （共 7 条）
反应条件
1: aq. Na2SO4 2: HCl View Scheme
参考文献
Sugihara,H. et al.
Justus Liebigs Annalen der Chemie, 1972 , vol. 763, p. 109 - 120
反应条件
potassium hydroxide; ethanol
参考文献
Will; Albrecht
Chemische Berichte, 1884 , vol. 17, p. 2103
参考文献
Sugihara,H. et al.
Justus Liebigs Annalen der Chemie, 1972 , vol. 763, p. 109 - 120
参考文献
Will; Albrecht
Chemische Berichte, 1884 , vol. 17, p. 2103
反应条件
1: 8.6 g / LAH / tetrahydrofuran / 24 h / Heating
2: conc. aq. HCl / 100 °C
View Scheme
参考文献
Jacob, Peyton; Shulgin, Alexander T.
Journal of Medicinal Chemistry, 1984 , vol. 27, # 7 p. 881 - 888
反应条件
1: 8.6 g / LAH / tetrahydrofuran / 24 h / Heating
2: conc. aq. HCl / 100 °C
3: 85 percent / dimethylformamide / 1 h / 100 °C
4: LiAlH4, 100percent H2SO4 / tetrahydrofuran / 1.5 h / Heating
View Scheme
参考文献
Jacob, Peyton; Shulgin, Alexander T.
Journal of Medicinal Chemistry, 1984 , vol. 27, # 7 p. 881 - 888
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Sugihara,H. et al.
Justus Liebigs Annalen der Chemie, 1972 , vol. 763, p. 109 - 120
