2,2,3,3-四(苯基)丁烷二腈合成路线 (共 37 条)
反应条件
methanol; sodium bromide in tetrahydrofuran T=20°C; 0.7 h; Electrolysis;
参考文献
Elinson, Michail N.; Ilovaisky, Alexey I.; Merkulova, Valentina M.; Zaimovskaya, Tatiana A.; Belyakov, Pavel A.; Nikishin, Gennady I.
Mendeleev Communications, 2010 , vol. 20, # 4 p. 207 - 208
反应条件
titanium tetrachloride in dichloromethane 1.) 0 deg C, 2.0 h, 2.) r.t., 2.5 h;
参考文献
Zieger, Herman E.; Wo, Shiming
Journal of Organic Chemistry, 1994 , vol. 59, # 14 p. 3838 - 3840
反应条件
titanium tetrachloride in dichloromethane 1.) 0 deg C, 2.0 h, 2.) r.t., 2.5 h;
参考文献
Zieger, Herman E.; Wo, Shiming
Journal of Organic Chemistry, 1994 , vol. 59, # 14 p. 3838 - 3840
反应条件
silver hexafluoroantimonate in dichloromethane 1.) -78 deg C, 20 min, 2.) -35 deg C, 1.5 h;
参考文献
Wo, Shiming; Zieger, Herman E.; Millar, Michelle M.; Koch, Stephen A.
Journal of Organic Chemistry, 1995 , vol. 60, # 18 p. 5925 - 5930
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide 2 h; Irradiation;
参考文献
Russell, Glen A.; Kulkarni, Shekhar V.; Khanna, Rajive K.
Journal of Organic Chemistry, 1990 , vol. 55, # 3 p. 1080 - 1086
反应条件
1-cyano-1-methylethylnitrate
参考文献
Emmons; Freeman
Journal of the American Chemical Society, 1955 , vol. 77, p. 4415
参考文献
Tsuge, Otohiko; Urano, Satoshi; Iwasaki, Takahiko
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 2 p. 485 - 489
反应条件
1: 93 percent / TiCl4 / CH2Cl2 / 2 h / 0 °C 2: 90 percent / TiCl4 / CH2Cl2 / 1.) 0 deg C, 2.0 h, 2.) r.t., 2.5 h View Scheme
参考文献
Zieger, Herman E.; Wo, Shiming
Journal of Organic Chemistry, 1994 , vol. 59, # 14 p. 3838 - 3840
反应条件
samarium diiodide in tetrahydrofuran 0.0333333 h; Title compound not separated from byproducts;
参考文献
Yacovan, Avihai; Hoz, Shmaryahu
Journal of Organic Chemistry, 1997 , vol. 62, # 3 p. 771 - 772
反应条件
di-tert-butyl peroxide 48 h; Heating;
参考文献
Lam, Yulin; Lee, Gene-Hsiang; Liang, Eping
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 6 p. 1033 - 1034