3-乙基-2-甲基苯并噻唑碘化物合成路线 （共 60 条）
反应条件
T=170°C; 0.333333 h; microwave irradiation;
参考文献
Winstead, Angela J.; Fleming, Nicole; Hart, Krystal; Toney, Deveine
Molecules, 2008 , vol. 13, # 9 p. 2107 - 2113
参考文献
Zhurnal Obshchei Khimii, , vol. 21, p. 2055,2056, 2061; engl. Ausg. S. 2295, 2301
反应条件
1: ethylquinaldinium iodide; N,N'-bis(4-methoxy-phenyl)formamidine With orthoformic acid triethyl ester in ethanol Heating; 2: With sulfonyl chloride resin; N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C; 3: 2-methyl-3-ethyl benzothiazolium iodide With pyridine; N-ethyl-N,N-diisopropylamine T=20°C; Further stages.;
参考文献
Mason, Stephen J.; Balasubramanian, Shankar
Organic Letters, 2002 , vol. 4, # 24 p. 4261 - 4264
反应条件
pyridine; triethylamine
参考文献
Oliveros,L.; Wahl,H.
Bulletin de la Societe Chimique de France, 1971 , p. 3204 - 3209
反应条件
pyridine; triethylamine; trichlorophosphate in acetic anhydride 0.5 h; Heating;
参考文献
Makin, S. M.; Pomogaev, A. I.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 10 p. 1916 - 1918
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 10 p. 2173 - 2176
参考文献
Oliveros,L.; Wahl,H.
Bulletin de la Societe Chimique de France, 1971 , p. 3204 - 3209
参考文献
Oliveros,L.; Wahl,H.
Bulletin de la Societe Chimique de France, 1971 , p. 3204 - 3209
反应条件
sodium acetate in acetic acid T=100°C; 1 h; Inert atmosphere;
参考文献
CANON KABUSHIKI KAISHA; SHINTOU, Taichi; NOMOTO, Tsuyoshi; WATANABE, Kohei; MIYAZAKI, Takeshi; TANAKA, Toshio; SHIMADA, Yasuhito; NISHIMURA, Yuhei
Patent: WO2014/65439 A1, 2014 ;
Location in patent: Paragraph 0163 ;
反应条件
triethylamine in acetic anhydride T=100°C; 0.333333 h;
参考文献
Gromov, S. P.; Razinkin, M. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 7.2 p. 1513
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , # 7 p. 1704
反应条件
2: pyridine View Scheme
参考文献
Kimura,S.
Bulletin of the Chemical Society of Japan, 1960 , vol. 33, p. 875 - 879
