5-乙基-2,4-二[(三甲基硅烷基)氧基]嘧啶合成路线 （共 7 条）
反应条件
in N,N-dimethyl-formamide 12 h; Heating;
参考文献
Mansuri; Ghazzouli; Chen; Howell; Brodfuehrer; Benigni; Martin
Journal of Medicinal Chemistry, 1987 , vol. 30, # 5 p. 867 - 871
反应条件
1,1,1,3,3,3-hexamethyl-disilazane in acetonitrile T=20°C;
参考文献
Miller; Pugh; Ullah; Gutteridge
Tetrahedron Letters, 2000 , vol. 41, # 51 p. 10099 - 10105
反应条件
in dichloromethane 6 h; Heating;
参考文献
Ubasawa; Takashima; Sekiya
Chemical and Pharmaceutical Bulletin, 1995 , vol. 43, # 1 p. 142 - 143
反应条件
trimethylsilyl trifluoromethanesulfonate in 1,2-dichloro-ethane; acetonitrile T=24°C; 3 h;
参考文献
Vorbrueggen, Helmut; Krolikiewicz, Konrad; Bennua, Baerbel
Chemische Berichte, 1981 , vol. 114, # 4 p. 1234 - 1255
反应条件
trimethylsilyl trifluoromethanesulfonate in 1,2-dichloro-ethane; acetonitrile T=24°C; 3 h;
参考文献
Vorbrueggen, Helmut; Krolikiewicz, Konrad; Bennua, Baerbel
Chemische Berichte, 1981 , vol. 114, # 4 p. 1234 - 1255
反应条件
1: 15.3 percent / (CH3)3SiOSO2CF3 / 1,2-dichloro-ethane; acetonitrile / 3 h / 24 °C 2: xylene / Heating 3: 27 percent / (CH3)3SiOSO2CF3 / acetonitrile; 1,2-dichloro-ethane / 46 h / 24 °C View Scheme
参考文献
Vorbrueggen, Helmut; Krolikiewicz, Konrad; Bennua, Baerbel
Chemische Berichte, 1981 , vol. 114, # 4 p. 1234 - 1255
反应条件
1: 1,2-dichloro-ethane / 1 h / 100 °C 2: sodium methoxide / methanol / 0.08 h / Heating View Scheme
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 46, # 4 p. 285 - 289
