2,2’-二氯二苯二硫醚合成路线 （共 15 条）
参考文献
Annali di Chimica (Rome, Italy), , vol. 44, p. 63,69
Bollettino Scientifico della Facolta di Chimica Industriale di Bologna, , vol. 13, p. 42,45
反应条件
1: bis-(2-chloro-phenyl)-disulfide With aluminium trichloride; zinc in acetonitrile T=80°C; 2 h; 2: diphenyliodonium(1+) iodide in water; acetonitrile T=80°C; 4.5 h;
参考文献
Movassagh, Barahman; Mossadegh, Amir
Phosphorus, Sulfur and Silicon and the Related Elements, 2005 , vol. 180, # 10 p. 2275 - 2278
反应条件
1: 1.) LDA / 1.) THF, -70 deg C, 1 h, 2.) THF, -70 deg C, 1 h 2: HCl (conc.) / 2 h / Ambient temperature View Scheme
参考文献
Tanaka, Hiromichi; Takashima, Hideaki; Ubasawa, Masaru; Sekiya, Kouichi; Nitta, Iasei; et al.
Journal of Medicinal Chemistry, 1992 , vol. 35, # 2 p. 337 - 345
反应条件
ytterbium; methyl iodide in tetrahydrofuran
T=25°C; 1 h;
参考文献
Su, Weike; Li, Yongshu; Zhang, Yongmin
Synthetic Communications, 2002 , vol. 32, # 14 p. 2101 - 2106
反应条件
CuO; potassium carbonate in N,N-dimethyl-formamide
T=140°C; 48 h; Inert atmosphereSchlenk technique;
参考文献
Rosario, Alisson R.; Casola, Kamila K.; Oliveira, Carla E.S.; Zeni, Gilson
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 14-15 p. 2960 - 2966
