2-(4-吗啉基)-1H-苯并咪唑合成路线 （共 9 条）
反应条件
sodium hydrogencarbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene in neat (no solvent) T=20°C; Green chemistry;
参考文献
Verma, Sanjeev K.; Acharya; Ghorpade, Ramarao; Pratap, Ajay; Kaushik
RSC Advances, 2013 , vol. 3, # 41 p. 18783 - 18786
反应条件
copper(l) iodide; caesium carbonate; N-methyl-2-(methylamino)ethylamine in N,N-dimethyl acetamide T=150°C; 16 h; Inert atmosphere;
参考文献
Deng, Xiaohu; McAllister, Heather; Mani, Neelakandha S.
Journal of Organic Chemistry, 2009 , vol. 74, # 15 p. 5742 - 5745
反应条件
copper(l) iodide; caesium carbonate; N-methyl-2-(methylamino)ethylamine in N,N-dimethyl acetamide T=150°C; 16 h; Inert atmosphere;
参考文献
Deng, Xiaohu; McAllister, Heather; Mani, Neelakandha S.
Journal of Organic Chemistry, 2009 , vol. 74, # 15 p. 5742 - 5745
反应条件
copper(l) iodide; caesium carbonate; N-methyl-2-(methylamino)ethylamine in N,N-dimethyl acetamide T=150°C; 16 h; Inert atmosphere;
参考文献
Deng, Xiaohu; McAllister, Heather; Mani, Neelakandha S.
Journal of Organic Chemistry, 2009 , vol. 74, # 15 p. 5742 - 5745
反应条件
copper(l) iodide; caesium carbonate; N-methyl-2-(methylamino)ethylamine in N,N-dimethyl acetamide T=150°C; 16 h; Inert atmosphere;
参考文献
Deng, Xiaohu; McAllister, Heather; Mani, Neelakandha S.
Journal of Organic Chemistry, 2009 , vol. 74, # 15 p. 5742 - 5745
反应条件
copper(l) iodide; caesium carbonate; N-methyl-2-(methylamino)ethylamine in N,N-dimethyl acetamide T=150°C; 16 h; Inert atmosphere;
参考文献
Deng, Xiaohu; McAllister, Heather; Mani, Neelakandha S.
Journal of Organic Chemistry, 2009 , vol. 74, # 15 p. 5742 - 5745
反应条件
T=95 - 100°C; 0.666667 h;
参考文献
Kuz'menko, V. V.; Nanavyan, I. M.; Pozharskii, A. F.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1992 , vol. 28, # 2 p. 154 - 157
Khimiya Geterotsiklicheskikh Soedinenii, 1992 , # 2 p. 190 - 193
反应条件
1: 35 percent / sodium hydroxylamine-O-sulfonate, NaOH / H2O / 1 h / 40 - 45 °C 2: 50 percent / N-bromosuccinimide / CH2Cl2 / 0.67 h / 5 - 10 °C 3: 80 percent / 0.67 h / 95 - 100 °C View Scheme
参考文献
Kuz'menko, V. V.; Nanavyan, I. M.; Pozharskii, A. F.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1992 , vol. 28, # 2 p. 154 - 157
Khimiya Geterotsiklicheskikh Soedinenii, 1992 , # 2 p. 190 - 193
参考文献
Kuz'menko, V. V.; Nanavyan, I. M.; Pozharskii, A. F.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1992 , vol. 28, # 2 p. 154 - 157
Khimiya Geterotsiklicheskikh Soedinenii, 1992 , # 2 p. 190 - 193
