(4-氟苯基)-磷酸二乙酯合成路线 （共 13 条）
反应条件
triethylamine; tetrakis(triphenylphosphine) palladium(0) T=20 - 90°C;
参考文献
PHARMACYCLICS, INC.
Patent: WO2007/87068 A2, 2007 ;
Location in patent: Page/Page column 103 ;
WO 2007/087068 A2
反应条件
n-butyllithium in tetrahydrofuran
参考文献
The United States of America as represented by the Secretary of the Navy
Patent: US6307098 B1, 2001 ;
反应条件
copper(I) oxide; 1,10-phenanthroline; N-ethyl-N,N-diisopropylamine in acetonitrile T=20°C; 24 h;
参考文献
Zhuang, Rongqiang; Xu, Jian; Cai, Zhenshi; Tang, Guo; Fang, Meijuan; Zhao, Yufen
Organic Letters, 2011 , vol. 13, # 8 p. 2110 - 2113
反应条件
nickel dichloride in neat (no solvent) T=160°C; Arbuzov Reaction; Microwave irradiation;
参考文献
Keglevich, Gyoergy; Gruen, Alajos; Boelcskei, Adrienn; Drahos, Laszlo; Kraszni, Marta; Balogh, Gyoergy T.
Heteroatom Chemistry, 2012 , vol. 23, # 6 p. 574 - 582
反应条件
palladium diacetate; caesium carbonate; potassium iodide in acetonitrile T=20 - 80°C; Inert atmosphere;
参考文献
Berrino, Roberta; Cacchi, Sandro; Fabrizi, Giancarlo; Goggiamani, Antonella; Stabile, Paolo
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 20 p. 4518 - 4520
反应条件
bis-triphenylphosphine-palladium(II) chloride; tetrabutyl-ammonium chloride; silver carbonate in dimethyl sulfoxide T=80°C; 9 h; Schlenk technique;
参考文献
Miao, Tao; Wang, Lei
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 5 p. 967 - 971
反应条件
sodium peroxodisulphate; silver nitrate in water; acetonitrile T=25°C; 48 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Effenberger, Franz; Kottmann, Hariolf
Tetrahedron, 1985 , vol. 41, # 19 p. 4171 - 4182
反应条件
phosphorus trichoride ueber mehrere Stufen;
参考文献
Jutisz et al.
Bulletin de la Societe Chimique de France, 1959 , p. 1551
反应条件
in ammonia T=-30°C; Irradiationcompetitive reaction, at known concentrations; relative rate constants, half life; Product distribution;
参考文献
Bunnett, Joseph F.; Mitchel, Eric; Galli, Carlo
Tetrahedron, 1985 , vol. 41, # 19 p. 4119 - 4132
反应条件
in tetrahydrofuran T=20°C; 4 h;
参考文献
European Journal of Inorganic Chemistry, , # 7 p. 1029 - 1034
