3,3'-二乙基硫代三碳菁碘化物合成路线 （共 13 条）
反应条件
1: With aniline in ethanol T=20°C; 0.0833333 h; 2: With sodium acetate in ethanol T=20°C;
参考文献
Okoh, Okoh Adeyi; Bisby, Roger H.; Lawrence, Clare L.; Rolph, Carole E.; Smith, Robert B.
Journal of Sulfur Chemistry, 2014 , vol. 35, # 1 p. 42 - 56
反应条件
acetic anhydride; triethylamine 1.) heating, 2.) room temp., 1h;
参考文献
Makin, S. M.; Kruglikova, R. I.; Shavrygina, O. A.; Kolobova, T. P.; Popova, T. P.; Tagirov, T. K.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 10 p. 1850 - 1852
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 10 p. 2093 - 2096
反应条件
acetic anhydride; triethylamine 1.) heating, 2.) room temp., 1h;
参考文献
Makin, S. M.; Kruglikova, R. I.; Shavrygina, O. A.; Kolobova, T. P.; Popova, T. P.; Tagirov, T. K.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 10 p. 1850 - 1852
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 10 p. 2093 - 2096
反应条件
acetic anhydride; triethylamine 1.) heating, 2.) room temp., 1h;
参考文献
Makin, S. M.; Kruglikova, R. I.; Shavrygina, O. A.; Kolobova, T. P.; Popova, T. P.; Tagirov, T. K.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 10 p. 1850 - 1852
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 10 p. 2093 - 2096
反应条件
acetic anhydride; triethylamine 1.) heating, 2.) room temp., 1h;
参考文献
Makin, S. M.; Kruglikova, R. I.; Shavrygina, O. A.; Kolobova, T. P.; Popova, T. P.; Tagirov, T. K.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 10 p. 1850 - 1852
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 10 p. 2093 - 2096
反应条件
1.1: toluene / 18 h / |Reflux 2.1: aniline / ethanol / 0.08 h / 20 °C 2.2: 20 °C View Scheme
参考文献
Journal of Sulfur Chemistry, , vol. 35, # 1 p. 42 - 56
反应条件
1.1: acetone / |Reflux 2.1: aniline / ethanol / 0.08 h / 20 °C 2.2: 20 °C View Scheme
参考文献
Journal of Sulfur Chemistry, , vol. 35, # 1 p. 42 - 56
反应条件
1.1: acetone / |Reflux 2.1: aniline / ethanol / 0.08 h / 20 °C 2.2: 20 °C View Scheme
参考文献
Journal of Sulfur Chemistry, , vol. 35, # 1 p. 42 - 56
反应条件
Multistep reaction. Title compound not separated from byproducts;
参考文献
Vompe, A. F.; Ivanova, L. V.; Meskhi, L. M.; Monich, N. V.; Raikhina, R. D.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 3 p. 529 - 537
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 3 p. 584 - 594
反应条件
T=300°C; Product distribution;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 18, # 2 p. 144 - 147
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 18, # 2 p. 188 - 192
