N-环己基丙-2-烯酰胺合成路线 （共 15 条）
反应条件
triethylamine in dichloromethane T=20°C; Cooling with ice;
参考文献
Tominey, Alan F.; Liese, Julia; Kraft, Arno; Wei, Sun; Kowski, Klaus; Schrader, Thomas
Beilstein Journal of Organic Chemistry, 2010 , vol. 6, art. no. 66
反应条件
silica supported sulfonic acid Ritter Amidation; 2 h; RefluxGreen chemistry;
参考文献
Mohammadi Ziarani, Ghodsi; Badiei, Alireza; Dashtianeh, Zeinab; Gholamzadeh, Parisa; Mohtasham, Nina Hosseini
Research on Chemical Intermediates, 2013 , vol. 39, # 7 p. 3157 - 3163
反应条件
sulfuric acid in chlorobenzene T=45 - 60°C; Ritter Amidation; 3.5 h;
参考文献
Chang, Sou-Jen
Organic Process Research and Development, 1999 , vol. 3, # 3 p. 232 - 234
参考文献
Chemische Fabrik Stockhausen and Cie.
Patent: US4237067 A1, 1980 ;
参考文献
Chemische Fabrik Stockhausen and Cie.
Patent: US4237067 A1, 1980 ;
反应条件
zeolite-HY in neat (no solvent) 1 h; Irradiation;
参考文献
Gadhwal, Sunil; Dutta, Manu Prakash; Boruah, Anima; Prajapati, Dipak; Sandhu, Jagir S.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1998 , vol. 37, # 8 p. 725 - 727
反应条件
potassium hydroxide; tetrabutylammomium bromide in tetrahydrofuran 0.5 h; Ambient temperature;
参考文献
Takahata, Hiroki; Ohnishi, Yoshinori; Yamazaki, Takao
Heterocycles, 1980 , vol. 14, # 4 p. 467 - 469
反应条件
1: 93 percent / Amberlite IR-120(H) resin 2: 24 percent / 1.) n-BuLi / 1.) DME, -78 degC to 25 degC, 130 min, 2.) 25 degC, 30 min View Scheme
参考文献
Adlington, R.M.; Barrett, A.G.M.
Tetrahedron, 1981 , vol. 37, # 23 p. 3935 - 3942
反应条件
aluminum oxide; phosphoric acid T=415°C;
参考文献
Eastman Kodak Co.
Patent: US2719175 , 1952 ;
参考文献
Wasserman,H.H. et al.
Tetrahedron Letters, 1979 , p. 549 - 552
