1: 17.01 g / LiAlH4 / diethyl ether / a) 10 deg C, 1 h, b) RT, 1 h 2: 36.05 g / pyridine / Ambient temperature 3: 6.01 g / NaBr / dimethylsulfoxide / 144 h / Ambient temperature View Scheme
参考文献
Takatsuto, Suguru; Watanabe, Tsuyoshi; Gotoh, Chiharu; Kuriyama, Hiroki; Noguchi, Takahiro; Fujioka, Shozo
Journal of Chemical Research, Miniprint, 1998 , # 4 p. 844 - 852
1: 24.41 g / LDA, HMPA / tetrahydrofuran / 2 h / -60 °C 2: 17.01 g / LiAlH4 / diethyl ether / a) 10 deg C, 1 h, b) RT, 1 h 3: 36.05 g / pyridine / Ambient temperature 4: 6.01 g / NaBr / dimethylsulfoxide / 144 h / Ambient temperature View Scheme
参考文献
Takatsuto, Suguru; Watanabe, Tsuyoshi; Gotoh, Chiharu; Kuriyama, Hiroki; Noguchi, Takahiro; Fujioka, Shozo
Journal of Chemical Research, Miniprint, 1998 , # 4 p. 844 - 852