2-甲基-5-苯基-1H-吡咯合成路线 (共 39 条)
反应条件
ammonia in methanol T=0 - 110°C; Paal-Knorr pyrrole synthesis; P=2625.26 Torr;
参考文献
Cranwell, Philippa B.; O'Brien, Matthew; Browne, Duncan L.; Koos, Peter; Polyzos, Anastasios; Pena-Lopez, Miguel; Ley, Steven V.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 30 p. 5774 - 5779
反应条件
tetrakis(triphenylphosphine) palladium(0); triethylamine in N,N-dimethyl-formamide T=80°C; 1 h;
参考文献
Tsutsui, Hironori; Narasaka, Koichi
Chemistry Letters, 1999 , # 1 p. 45 - 46
反应条件
triethylamine; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=80°C; tandem amino-Heck carbonylation; P=760.051 Torr; 2 h;
参考文献
Zaman, Shazia; Kitamura, Mitsuru; Abell, Andrew D.
Australian Journal of Chemistry, 2007 , vol. 60, # 8 p. 624 - 626
反应条件
triethylamine; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=90°C; amino-Heck reaction; 2 h;
参考文献
Zaman, Shazia; Kitamura, Mitsuru; Abell, Andrew D.
Australian Journal of Chemistry, 2007 , vol. 60, # 8 p. 624 - 626
反应条件
C29H46IrN5P2; potassium tert-butylate in tetrahydrofuran T=90°C; 24 h;
参考文献
Qu, Shuanglin; Dang, Yanfeng; Song, Chunyu; Wen, Mingwei; Huang, Kuo-Wei; Wang, Zhi-Xiang
Journal of the American Chemical Society, 2014 , vol. 136, # 13 p. 4974 - 4991
反应条件
FeC2O4·2H2O; pyclen T=130°C; Suzuki-Miyaura reaction; 10 h; regioselective reaction;
参考文献
Wen, Jun; Qin, Song; Ma, Li-Fang; Dong, Liang; Zhang, Ji; Liu, Shan-Shan; Duan, Yi-Shu; Chen, Shan-Yong; Hu, Chang-Wei; Yu, Xiao-Qi
Organic Letters, 2010 , vol. 12, # 12 p. 2694 - 2697
反应条件
potassium hydroxide in dimethyl sulfoxide T=140°C; 4 h;
参考文献
Aliev, I. A.; Gasanov, B. R.; Zeinalova, S. N.; Mikhaleva, A. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, p. 1954 - 1955
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 9 p. 2175 - 2177
反应条件
in dichloromethane T=0°C; 1.25 h; Irradiation;
参考文献
Ito, Masato M.; Nomura, Yujiro; Takeuchi, Yoshito; Tomoda, Shuji
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 2 p. 533 - 536
反应条件
(NH4)2CO3 in N,N-dimethyl-formamide Kornblum-de la Mare rearrangement;
参考文献
Hewton, Cassie E; Kimber, Marc C; Taylor, Dennis K
Tetrahedron Letters, 2002 , vol. 43, # 17 p. 3199 - 3201
反应条件
methanol; potassium hydroxide 72 h; RefluxInert atmosphere;
参考文献
Barber, David M.; Sanganee, Hitesh; Dixon, Darren J.
Chemical Communications, 2011 , vol. 47, # 15 p. 4379 - 4381