2-氨基-3,6-二氯苯甲酸合成路线 （共 13 条）
反应条件
dihydrogen peroxide; sodium hydroxide in water T=50°C; 0.5 h; Inert atmosphereSchlenk technique;
参考文献
Chang, Ning-Hui; Chen, Xi-Chao; Nonobe, Hikaru; Okuda, Yasuhiro; Mori, Hiroki; Nakajima, Kiyohiko; Nishihara, Yasushi
Organic Letters, 2013 , vol. 15, # 14 p. 3558 - 3561
反应条件
1: hydroxylamine hydrochloride; sodium sulfate / water; ethanol / 12 h / 80 °C / |Inert atmosphere; |Schlenk technique 2: sulfuric acid / water / 0.25 h / 100 °C / |Inert atmosphere; |Schlenk technique 3: sodium hydroxide; dihydrogen peroxide / water / 0.5 h / 50 °C / |Inert atmosphere; |Schlenk technique View Scheme
参考文献
Organic Letters, , vol. 15, # 14 p. 3558 - 3561
反应条件
1: sulfuric acid / water / 0.25 h / 100 °C / |Inert atmosphere; |Schlenk technique 2: sodium hydroxide; dihydrogen peroxide / water / 0.5 h / 50 °C / |Inert atmosphere; |Schlenk technique View Scheme
参考文献
Organic Letters, , vol. 15, # 14 p. 3558 - 3561
参考文献
Chemische Berichte, , vol. 34, p. 1338
参考文献
Zhurnal Obshchei Khimii, , vol. 23, p. 606,609; engl. Ausg. S. 629, 632
反应条件
2: AlCl3; NaCl 3: aqueous NaOH View Scheme
参考文献
Zhurnal Obshchei Khimii, , vol. 23, p. 606,609; engl. Ausg. S. 629, 632
反应条件
1: AlCl3; NaCl 2: aqueous NaOH View Scheme
参考文献
Zhurnal Obshchei Khimii, , vol. 23, p. 606,609; engl. Ausg. S. 629, 632
参考文献
Chemische Berichte, , vol. 28, p. 1385
参考文献
Chemische Berichte, , vol. 33, p. 2024
参考文献
Graebe; Gourevitz
Chemische Berichte, 1900 , vol. 33, p. 2024
